Investigation of Carbon Fibre Reinforced Composites Based on Novel Phenylethynyl-Terminated Polyimde

Article Preview

Abstract:

As part of the continuing studies to develop high performance composite based on new kind of phenylethynyl end-capped imide oligomers for aerospace applications, PETI-type polyimide composites were prepared from carbon fibre (CF) and polyimide matrix resin derived from dianhydride (s-BPDA), 2,5-bis(4-aminophenoxy)-biphenyl(p-TPEQ) and 4-phenylethynylphthalic anhydride (PEPA). The mechanical properties were tested at both room temperature and 177 °C. The flexural properties were determined by 3-point-bending at room temperature. Thermal aging test was carried out by exposing samples at 177°C over 1000 hours, and the mechanical properties were also evaluated before and after isothermal aging. It was demonstrated that the composite had good thermal and mechanical properties.

You might also be interested in these eBooks

Info:

Periodical:

Advanced Materials Research (Volumes 415-417)

Pages:

310-315

Citation:

Online since:

December 2011

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2012 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

[1] Meador M A 1998 Annu. Rev. Mater. Sci. 28 599

Google Scholar

[2] Harris, F. W.; Sridhar, K.; Das, S. Polyimide Oligomers Terminated with Thermally-Polymerizable Groups. ACS Div. Polym. Chem., Polym.Prepr. 1984, 25(1), 110-111

Google Scholar

[3] Harris, F. W.; Pamidimukkala, A.; Gupta, R.; Das, L.; Wu, T.; Mock, G. Syntheses and Characterization of Reactive End-Capped PolyimideOligomers. J. Macromol. Sci., Chem. 1984, A21(8&9), 1117-1135

DOI: 10.1080/00222338408056595

Google Scholar

[4] Paul, C. W.; Schultz, R. A.; Fenelli, S. P. Polyimides End-Capped with Diaryl Substituted Acetylene; Composites, Molding Material, Adhesives, Electronics. US Pattent 5,138,028, Aug 11, 1992. In Advacnes in Polyimide Science and Technology, Feger, C., Khoyastech, M. M., Htoo, M.S., Eds.; Technomic: Lancaster, PA, 1993; pp.220-244.

Google Scholar

[5] Hergenrother, P. M.; Bryant, R. G.; Jensen, B. J.;Havens, S. J. Phenyl ethynyl-Terminated Imide Oligomers and Polyers Therefrom. J. Polym. Sci., Part A: Polym. Chem. 1994, 32, 3061-3067

DOI: 10.1002/pola.1994.080321607

Google Scholar

[6] Hergenrother, P. M.; Smith, J. W., Jr. Chemistry and Properties of Imide Oligomer End-Capped with Phenylethynylphthalic Anhydrides. Polymer 1994, 35,4857-4864

DOI: 10.1016/0032-3861(94)90744-7

Google Scholar

[7] Connell JW, Smith Jr JG, Hergenrother PM. JMS Rev Macromol Chem Phys 2000;C40(2&3):207-30.

Google Scholar

[8] Fang X, Rogers DF, Scola DA, Stevens MP. J Polym Sci Part A Polym Chem 1998;36:461.

Google Scholar

[9] Xianhua Rao, Hongwei Zhou, Guodong Dang, Chunhai Chen, Zhongwen Wu. Polymer 47 (2006) 6091-6098

Google Scholar

[10] Wilson D. Polyimides as resin matricies for advanced composites. In: Wilson D, Stenzenberger HD, Hergenrother PM, editors. Polyimides. Glasgow, New York: Chapman and Hall, Blackie; 1990. p.187–226.

DOI: 10.1007/978-94-010-9661-4_7

Google Scholar

[11] Bowles K J 1993 SAMPE Q. 24, 49

Google Scholar

[12] Toshio Ogasawara a, Yuichi Ishida a, Rikio Yokota a, Toshitaka Watanabe b, Tatsuji Aoi b, Jun Goto b Composites: Part A 38 (2007) 1296–1303

Google Scholar