Shape-Controlled Pd Nanoparticles in the Mixed Surfactants by Ultrasonic Irradiation

Yan Li Wang; Ming Xu Zhang; De Xin Tan

doi:10.4028/www.scientific.net/AMR.430-432.655

Paper Titles

Evaluation on Chloride Cracking of S135 High-Strength Drill Pipe
p.636

Analysis of Elastic Moduli and Fracture of Concrete with Nature Element Method in Mesoscale
p.640

Preparation and Characterization of MicroPCMsContaining Paraffin
p.647

Numerical Simulation of Spraying and Jointing for Polyurea Spraying Gun
p.651

Shape-Controlled Pd Nanoparticles in the Mixed Surfactants by Ultrasonic Irradiation
p.655

Prediction of Cutting Consumption Based on Optimization-Making RBF Artificial Neural Network
p.659

Model and Analysis of Flexural Properties of Al₂O₃ Ceramic Prepared by Centrifugal Slip Casting Using BP Neural Network Model
p.664

Strip Casting of Al-25%Si Alloy
p.669

Construction of a Museum: An Example of Cultural Education
p.673

HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 430-432Shape-Controlled Pd Nanoparticles in the Mixed...

Shape-Controlled Pd Nanoparticles in the Mixed Surfactants by Ultrasonic Irradiation

Abstract:

nanoPd nanoparticles were prepared using ultrasonic irradiation in the PdCl₂/H₂O/EtOH solution by the addition of a quantity of hexadecyl trimethyl ammonium bromide (CTAB) and sodium dodecyl sulfonate (SDS) . The products were characterized by XRD、TEM and low temperature nitrogen adsorption-desorption. The effects of the composition of CTAB and SDS on the growth morphology of palladium nanoparticles were investigated. The results indicate that the size and morphology of the nanoPd particles were controllable by adjusting the ratio of CTAB and SDS. The polygonal nanoPd particles with a distributed size of 10-20 nm were obtained when the molar ratio of CTAB:SDS was 1:1 and the reaction time was 60min. The nanoparticles obtained by addition of two surfactants (CTAB and SDS) increased the BET surface area by 14 m²∙g^-1 compared to that obtained without surfactant.