Research on Detecting Tris-(2,3-dibromopropyl)-Phosphate in Textiles with the HPLC/DAD Method

Ke Jie Fu; Li Sheng Yang; Chang Sheng Feng; Liang Chen

doi:10.4028/www.scientific.net/AMR.441.640

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Research on Detecting Tris-(2,3-dibromopropyl)-Phosphate in Textiles with the HPLC/DAD Method
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HomeAdvanced Materials ResearchAdvanced Materials Research Vol. 441Research on Detecting...

Research on Detecting Tris-(2,3-dibromopropyl)-Phosphate in Textiles with the HPLC/DAD Method

Abstract:

A detecting method for toxic flame retardant finishing agent tris-(2,3-dibromopropyl) -phosphate (TRIS for short) in textiles was studied. In the method, an acetonitrile ultrasound-assisted extraction process was included in sample pre-treatment, and HPLC/DAD was used in the separation and identification of extractives. After that, the conditions of pre-treatment and chromatograph were optimized. The results showed that the limit of detection (LOD) by this method (S/N10) is 1.0 mg/kg, its recovery ranged from 78.1% to 98.4%, and RSD of the precision test is 3.2%, of which all met the requirements for routine testing.

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Periodical:

Advanced Materials Research (Volume 441)

Pages:

640-644

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.441.640

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Online since:

January 2012

Authors:

Ke Jie Fu, Li Sheng Yang, Chang Sheng Feng, Liang Chen

Keywords:

Detecting, Flame Retardant, HPLC/DAD, Textile, Tris-(2,3-Dibromopropyl)-Phosphate

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