Synthesis of Well-Dispersed Copper Nanoparticles by L-Ascorbic Acid in Diethyleneglycol

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Metallic copper nanoparticles were synthesized in the presence of poly(N-vinylpyrrolidone) (PVP) as the capping agent and L-ascorbic acid as the reducing agent in diethyleneglycol (DEG) solvent. The obtained copper nanoparticles were characterized by scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), transmission electron microscopy (TEM) and X-ray diffraction (XRD). The EDS and XRD results showed that the resultant particles were confirmed to be crystalline Cu with a face-centered cubic (fcc) structure. It was also observed that the diameter of obtained copper particles ranging from 80 to 120nm via SEM and TEM.

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378-381

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July 2012

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© 2012 Trans Tech Publications Ltd. All Rights Reserved

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[1] W. P. Halperin: Rev. Mod. Phys. Vol. 58 (1986), p.533.

Google Scholar

[2] J. H. Fendler.: Chem. Rev. Vol. 87 (1987), p.877.

Google Scholar

[3] N. A. Dhas, C. P. Raj and A. Gedanken: Chem. Mater. Vol. 10 (1998), p.1446.

Google Scholar

[4] H.H. Huang, F.Q. Yan and Y.M. Kek: Langmuir Vol. 13 (1997), p.172.

Google Scholar

[5] Z. Liu and Y. Bando: Adv. Mater. Vol. 15 (2003), p.303.

Google Scholar

[6] S. Jeong, H.C. Song and W.W. Lee: Langmuir Vol. 27 (2011), p.3144.

Google Scholar

[7] K. Woo, D. Kim and J.S. Kim: Langmuir Vol. 25 (2009), p.429.

Google Scholar

[8] I.G. Casella, T.R.I. Cataldi and A. Guerrieri: Anal. Chim. Acta Vol. 335 (1996), p.217.

Google Scholar

[9] M.S. Yeh, Y.S. Yang and Y.P. Lee: J. Phys. Chem. B Vol. 103 (1999), p.6851.

Google Scholar

[10] R.V. Kumar, Y. Mastai and Y. Diaman: J. Mater. Chem. Vol. 11 (2001), pp.1-209.

Google Scholar

[11] Z.W. Liu and Y. Bando: Adv. Mater. Vol. 15 (2003), p.303.

Google Scholar

[12] S. Jeong, K. Woo and D. Kim: Adv. Funct. Mater. Vol. 18 (2008), p.679.

Google Scholar

[13] F. Bonet, V. Delmas and S. Grugeon: Nanostruct. Mater. Vol. 11 (1999), p.1277.

Google Scholar

[14] H.X. Zhang, U. Siegert and R. Liu: Nanoscale Res. Lett. Vol. 4 (2009), p.705.

Google Scholar

[15] I. Pastoriza-Santos and L.M. Liz-marzan: Langmuir Vol. 15 (1999), p.948.

Google Scholar

[16] Y.W. Tan, X.H. Dai and Y.F. Li: J. Mater. Chem. Vol. 13 (2003), p.1069.

Google Scholar

[17] K.S. Chou, C.Y. Lee and N.E. Stot: Nanotechnology Vol. 194 (2008), p.15604.

Google Scholar

[18] X.F. Tang, Z.G. Yang and W.J. Wang: Colloids and Surfaces A: Physicochemical and Engineering Aspects Vol. 360 (2010), p.99.

Google Scholar

[19] N. Leopold and B. Lendl: J. Phys. Chem. B Vol. 107 (2003), p.5723.

Google Scholar