Experimental Research on Separation of Benzoic Acid Residua by Vacuum Distillation

Feng Wei; Liang He; Hua Li; Pei Hua Shi

doi:10.4028/www.scientific.net/AMR.550-553.970

Paper Titles

The Relationship between Elemental Form of Solid Phase and COS Formation over MnO_X Desulfurization Sorbent
p.953

Deep Desulfurization of Model Oil Using Ionic Liquid and Active Carbon Binary System
p.957

Studies on CO₂ Absorption in Simulating Flue Gas
p.961

Enhanced Adsorption of Methyl Orange on Mesoporous TiO_2-XC_X Modified by CTAB
p.966

Experimental Research on Separation of Benzoic Acid Residua by Vacuum Distillation
p.970

The Performance Research on Reaction of Fe₂O₃/Al₂O₃ Oxygen Carrier and CO in Chemical-Looping Combustion Process
p.974

CFD-DPM Modeling of Gas-Liquid Flow in a Stirred Vessel
p.979

Study on Macroporous Resin Separation and Purification of Total Flavonoids of Plantago Process
p.987

Physical Properties of Chitosan Edible Films Incorporated with Essential Oil Monomers
p.993

HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 550-553Experimental Research on Separation of Benzoic...

Experimental Research on Separation of Benzoic Acid Residua by Vacuum Distillation

Abstract:

The fractions of benzyl benzoate and fluorenone were enriched from the benzoic acid residua by flash separation. Then this fraction was separated by vacuum batch distillation. The recovery of benzoic acid residua was implemented. The experiment proves this method is feasible. And purity about 90% of benzyl benzoate and more than 85% of fluorenone products were obtained. Simultaneously the study analyzed the impact of tower top pressure, tower top and bottom temperature, reflux ratio on product purity. The optimal condition in operating was defined in the experiment condition.