Hydrothermal Synthesis of Tetragonal Phase CuInS2 Nanoparticles

Zhi Xin Chen; Ya Zhen Ye; Han Jie Huang; Guang Can Xiao; Yun Hui He

doi:10.4028/www.scientific.net/AMR.557-559.489

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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 557-559Hydrothermal Synthesis of Tetragonal Phase CuInS2...

Hydrothermal Synthesis of Tetragonal Phase CuInS₂ Nanoparticles

Abstract:

The tetragonal phase CuInS₂ nanoparticles were synthesized by the reaction of Cu(Ac)₂, InCl₃·4H₂O and thioacetamide by hydrothermal method at 200 °C for 6 h in pH 1. The products were characterized by X-ray diffraction, energy-dispersive X-ray spectrum, X-ray photoelectron spectroscopy, scanning electron microscopy (SEM) and transmission electron microscopy (TEM) techniques. Experimental results indicate that reaction temperature and the pH of solution are the important factors in the formation of CuInS₂. The SEM and TEM results illuminated that the CuInS₂ was composed of so many nanoparticles.

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Periodical:

Advanced Materials Research (Volumes 557-559)

Pages:

489-492

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.557-559.489

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Online since:

July 2012

Authors:

Zhi Xin Chen, Ya Zhen Ye, Han Jie Huang, Guang Can Xiao, Yun Hui He

Keywords:

CuInS₂, Hydrothermal, Nanoparticle, Tetragonal Phase

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