Analysis of Volatile Compounds in Flowers of Akebia trifoliata by Headspace Solid-Phase Microextraction Coupled to Gas Chromatography-Mass Spectrometry

Abstract:

Objective: To analyse chemical constituents of the volatiles flowers of Akebia trifoliata. Method: The volatiles of bungei were extracted through Headspace solid-phase microextracti, and then the constituents were separated by GC and identified by MS. Result and Conclusion: 22 Compounds were identified. The principal chemical constituents of the volatiles flowers of Akebia trifoliata are α- Farnesene and Farnesene*(80.827%），Ocimene and Ocimene* （14.699%）、πPatchoulene and πPatchoulene*(1.200%) etc,respectively.

• Periodical: Advanced Materials Research (Volumes 602-604)
• Pages: 1313-1316
• DOI: https://doi.org/10.4028/www.scientific.net/AMR.602-604.1313
• Online since: December 2012
• Authors: Ting Xiao*, Le Wang, Ting Liu, Ai Nong Yu, Xiao Hong Yang
• Keywords: Akebia trifoliata, Chemical Composition, Gas Chromatography-Mass Spectrometry (GC-MS), Headspace Solid-Phase Microextraction, Volatiles Oil

References

[1] Chinese Pharmacopoeia Commission. Pharmacopoeia of people's Republic of China [M]. Beijing: Chemical Industry Press，2005.

[2] XIE X X,GE F H. Study on Supercritical CO2 Extraction of Fatty Oils from the Seed of Akebia trifoliata(Thunb)Koidz[J].Journal of Chinese Medicinal Materials,2007,30(3):345-349.

[3] KONG J.Chemical constituents and medical activity Decaisnea[J].J.Northwest Normal University, 1996,32(3):108-111.

[4] ZHENG Q A,YANG CH R.Chemotaxonomic study on the family of Lardizabalaceae[J].Chinese Bulletin Botany,2001,18(3):332-339.

[5] LIU G Y,WANG Y,MA SH CH,et al. Chemical constituents and biological activities of Akebia Decne.[J].Chin.Pharm.J.，2004，39(5):330-332.

[6] WANG Y,LU J,LIN R CH. Study on the chemical constituents from rattan of Akebia trifoliata[J].Chinese Traditional and Herbal Drugs，2004，35(5):495-498.

[7] YANG J SH ,CHEN D ZH. China flora. Vol. twenty-ninth. Beijing: Science Press，2001：4.

[8] CAO L，Determination of Trace Elements of Akebia trifoliate in Jiangxi Wuyuan[J].Lishizhen medicine and materia medica research，2008，19（3）:544-545.

[9] ZHANG Q,TANG N.N,YU H.L.et al. Yulan fruit fatty acid composition analysis of GC-MS [J]. Journal of Henan University, 2009, 28 (2): 101-103.

[10] CHEN X.R.,WEI C.H. Research on Chemical Composition of Lotus and Magnolia Flower[J]. Chinese Medicine, 2003, 23(3): 159-161.

[11] CHEN ZH.H. Study on Essence Oils from Hedychium Coronarium by Microwave Method[J]. Lishizhen Medicine and Materia Medica Research, 2005, 16 (7): 613-614.

[12] XIE J CH,SUN B G,YU M.Analysis of Volatiles in the Leaf and Stem of Fragrant Plant Vitex negundo L.var.heterophylla（Franch.）Rehd[J].Food and fermentation industries，2005，31(7): 100-103

[13] XIE J CH,SUN B G,ZHENG F P,et al. Components of Extract from Leaf or Stem of Vitex negundo L. vat.heterophylla（Franch.） Rehd.by Supercritical CO2 Fluid[J].Food Science，2005, 26(8):281-283.

[14] NA ZH.Red axe leaf chemical components of the essential oil [J].Fragrance flavor and cosmetic，2008，6：26-27