Preparation, Characterization of N-Ti-MCM-22 Molecular Sieve and its Photocatalytic Properties

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Abstract:

Nanocrystalline N-doped and Ti-containing MCM-22 catalyst was synthesized by the static hydrothermal method, using sodium azide as nitrogen source for doping, and tetra-n-butyl titanate [Ti(OC4H9)4] as precursors of TiO2. The catalysts were characterized by X-ray diffraction, transmission electron microscopy, and energy-dispersive spectroscopy.During liquid phase photocatalytic degradation of methylene blue (MB) under high-pressure Hg arc lamp irradiation, the asprepared N-doped Ti-MCM-22 exhibited much higher activity than the undoped Ti-MCM-22, attributed to the effect of nitrogen dopant.

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Advanced Materials Research (Volumes 602-604)

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205-208

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December 2012

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© 2013 Trans Tech Publications Ltd. All Rights Reserved

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