Thermal Degradation and Microhardness Analysis of Polyene with Modified Oil Resin

Mohd Nurazzi Norizan; Rahmah Mohamed; Ahmad Faiza Mohamad

doi:10.4028/www.scientific.net/AMR.664.590

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HomeAdvanced Materials ResearchAdvanced Materials Research Vol. 664Thermal Degradation and Microhardness Analysis of...

Thermal Degradation and Microhardness Analysis of Polyene with Modified Oil Resin

Abstract:

Thermal degradation of polyene synthesized from recycle polyvinyl chloride (PVC) and hardness of polyene coated with modified oil has been studied by thermogravimetric analysis (TGA) and microhardness test. The synthesized polyene from reaction of recycle PVC were varied from 30 minutes, 1 hour, 2 hours and 4 hours and their thermal stability has been analyzed. From differential thermal gravimetric, DTG curve, polyene from two hours reaction showed the highest degradation temperature up to 445°C due to degradation of polyene sequences. Microhardness test performed by Shimadzu DUH 211/DUH-211S dynamic ultra microhardness tester according to ASTM E384 showed that polyene derived from 2 hours PVC with modifed oil resin resulted in the highest microhardness ~ 107.99 MPa.

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Periodical:

Advanced Materials Research (Volume 664)

Pages:

590-595

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.664.590

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Online since:

February 2013

Authors:

Mohd Nurazzi Norizan, Rahmah Mohamed, Ahmad Faiza Mohamad

Keywords:

Degradation Temperature, Fourier Transform Infrared Spectroscopy (FTIR), Micro-Hardness Test, Polyene

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