An Easy Way to Synthesize YAG Nanoparticles for Transparent Ceramics via Allegro Vacuum Freeze Drying

Article Preview

Abstract:

In this paper, high purity, weak agglomerated, well crystallized and dispersed YAG nanoparticles were prepared by Allegro vacuum freeze drying which included solution preparation, allegro freezing, freeze drying and calcination. The results showed that the precursor directly converted into pure YAG at 900°C and no intermediate phase was found. Considering the crystallinity and dispersion, the best calcination temperature was 1100°C.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

203-207

Citation:

Online since:

June 2013

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2013 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

[1] Ikesue A, Kinoshita T, Kamata K, Yoshida K, Fabrication and optical properties of high-performance polycrystalline Nd: YAG ceramics for solid-state lasers, J Am Ceram Soc. 78.

DOI: 10.1002/chin.199535309

Google Scholar

[4] (1995)1033-1040.

Google Scholar

[2] Jiang LI, Yusong WU, Yubai PAN et al, Solid-state-reaction fabrication and properties of a high-doping Nd: YAG transparent laser ceramic, Front. Chem. Eng. China 2 (2008) 248-252.

DOI: 10.1007/s11705-008-0048-6

Google Scholar

[3] Zhihong Sun, Duorong Yuan, Haoqiang Li et al, Synthesis of yttrium aluminum garnet (YAG) by a new sol-gel method, Journal of Alloys and Compounds 379 (2004) L1-L3.

DOI: 10.1016/j.jallcom.2004.02.030

Google Scholar

[4] Jahangir Hasani Barbaran, Morteza Farmahini Farahani, Fereshteh Hajiesmaeilbaigi, Synthesis of highly doped Nd: YAG powder by SOL-GEL method, Semiconductor Physics, Quantum Electronics & Optoelectronics, 8.

Google Scholar

[1] 2005) 87-89.

Google Scholar

[5] L. D. Wang, L. G. Zhang, Y. Fan, J. S. Luo, P. P. Zhang, and L. N. An, Synthesis of Nd/Si Codoped YAG Powders Via a Solvothermal Method, J. Am. Ceram. Soc. 89.

DOI: 10.1111/j.1551-2916.2006.01261.x

Google Scholar

[11] (2006) 3570-3572.

Google Scholar

[6] J. W. G. A. Vrolijk, J. W. M. M. Willems, and R. Metselaar, Co-precipitation of Yttrium and Aluminum Hydroxides for Preparation of Yttrium Aluminum Garnet, J. Eur. Ceram. Soc. 6 (1990) 47-51.

DOI: 10.1016/0955-2219(90)90034-d

Google Scholar

[7] P. Palmero, C. Esnouf, L. Montanaro, and G. Fantozzi, Influence of the Co-Precipitation Temperature on Phase Evolution in Yttrium-Aluminium Oxide Materials, J. Eur. Ceram. Soc. 25 (2005) 1565-1573.

DOI: 10.1016/j.jeurceramsoc.2004.05.027

Google Scholar

[8] J. G. Li, T. Ikegami, J. H. Lee, T. Mori, and Y. Yajima, Co-precipitation Synthesis and Sintering of Yttrium Aluminum Garnet (YAG) Powders: The Effect of Precipitant, J. Eur. Ceram. Soc. 20 (2000) 2395-2405.

DOI: 10.1016/s0955-2219(00)00116-3

Google Scholar

[9] Y. Rabinovitch, C. Bogicevic, F. Karolak, and et al, Freeze-dried nanometric neodymium-doped YAG powders for transparent ceramics, Journal of Materials Processing Technology. 99 (2008) 314-320.

DOI: 10.1016/j.jmatprotec.2007.08.022

Google Scholar

[10] Hua Gong, Ding-yuan Tang, and Hui Huang, Agglomeration control of Nd: YAG nanoparticles via Freeze drying for transparent Nd: YAG ceramics, J. Am. Ceram. Soc. 92.

Google Scholar

[4] ( 2009) 812-817.

Google Scholar

[11] M. B. KAKADE, S. RAMANATHAN, S. K. ROY,Synthesis of YAG powder by aluminum nitrate yttrium nitrate glycine reaction,Journal of Materials Science Letters 21(2002) 927- 929.

Google Scholar

[12] LI Chang-qing, ZUO Hong-bo, ZHANG Ming-fu, and et al, Fabrication of transparent YAG ceramics by traditional solid-state-reaction method. Trans. Nonferrous Met. Soc. China 17(2007) 148-153.

DOI: 10.1016/s1003-6326(07)60064-8

Google Scholar