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Synthesis and Rheological Properties of Poly (AM-TBAM-NMMAD) Random-Block Copolymer

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Abstract:

Poly (TBAM-AM-NMMAD) random-block copolymer were prepared by aqueous micellar copolymerization using AIBA (V50), ammonium persulfate (J) and sodium bisulfite (D) as initiator and SDS as surfactant in the mixture solvent of deionized water. The structure of Poly (TBAM-AM-NMMAD) was characterized by solid state 13C-NMR and FTIR spectroscopy and the dynamic viscosity was measured by the NDJ-1 viscometer. The experimental results and analysis shows poly (AM-TBAM-NMMAD) random-block copolymer which had been endowed with high rheological properties was successfully synthesized by controlling the abundance of initiator based on the method of orthogonal experiment.

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Periodical:

Advanced Materials Research (Volumes 712-715)

Pages:

190-194

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.712-715.190

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Online since:

June 2013

Authors:

Ya Qian Wu, Xue Feng Shi, Feng Zhao, Nan Ye Ying

Keywords:

Dynamic Viscosity, Initiator, Orthogonal Experiment, Poly(TBAM-AM-NMMAD)

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© 2013 Trans Tech Publications Ltd. All Rights Reserved

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