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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 726-731Hollow Fiber Liquid Phase Microextraction as an...

Hollow Fiber Liquid Phase Microextraction as an Advantageous Approach for Preconcentraton of Malachite Green in Environmental Water

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Abstract:

A two-phase hollow fiber liquid phase microextraction (HF-LPME) by coupling with high performance liquid chromatography (HPLC) was developed to analyze malachite green (MG) in environmental water. In this method, 1-octyl-3-methylimidazolium hexafluorophosphate ([C₈MI[PF₆]) was selected as extraction agent, and several parameters (sample pH, salinity, extraction time, shaking rate, volume of donor phase) that could affect extraction performance were investigated. Under the optimal extraction conditions (sample pH, 5; salinity, 4% sodium chloride; extraction time, 6 h; shaking rate, 200 rpm; volume of donor phase, 200 mL), the established method showed excellent characters as: high enrichment factor (1193), wide linear range (0.2-100 μg L^-1), low detection limit (0.1 μg L^-1), good reproducibility (relative standard deviation, RSD 8.4%, n= 5) and satisfactory recovery (102.8%, n= 5). The approach was applied in real water samples analysis, which indicated that it has great potentials for rapidly monitoring low concentration of MG in environmental waters.

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Advances in Environmental Technologies

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Periodical:

Advanced Materials Research (Volumes 726-731)

Pages:

1491-1495

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.726-731.1491

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Online since:

August 2013

Authors:

Zhen Chang*, Kai Zhou, Liu Qing Yang, Xiang Yang Wu, Zhen Zhang

Keywords:

Environmental Water, Hollow Fiber Liquid Phase Microextraction, Ionic Liquid (IL), Malachite Green

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© 2013 Trans Tech Publications Ltd. All Rights Reserved

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[1] S. Srivastava, R. Sinha and D. Roy: Aquat. Toxicol. Vol. 66 (2004), p.319

[2] K. Mitrowska, A. Posyniak and J. Zmudzki: Anal. Chim. Acta. Vol. 586 (2007), p.420

[3] K. Mitrowska, A. Posyniak and J. Zmudzki: J. Chromatogr. A. Vol. 1089 (2005), p.187

[4] I. Safarik and M. Safarikova: Water Res. Vol. 36(2002), p.196

[5] A. A. Bergwerff and P. Scherpenisse: J. Chromatogr. B Analyt. Technol. Biomed Life Sci. Vol. 788 (2003), p.351

[6] Z. Guo, P. Gai, T. Hao, J. Duan and S. Wang: J. Agric. Food Chem. Vol. 59 (2011), p.5257

[7] N. Pourreza and S. Elhami: Anal. Chim. Acta, Vol. 596 (2007), p.62

[8] L. An, J. Deng, L. Zhou, H. Li, F. Chen, H. Wang and Y. Liu: J. Hazard. Mater. Vol. 175 (2009), p.883

[9] M. A. Pierrard, P. Kestemont, E. Delaive, M. Dieu, M. Raes and F. Silvestre: Aquat. Toxicol. Vol. 114-115 (2012), p.142

DOI: 10.1016/j.aquatox.2012.02.020

[10] F. Ding, X. N. Li, J. X. Diao, Y. Sun, L. Zhang, L. Ma and X. L. Yang: Ecotoxicol. Environ. Saf. Vol. 78 (2012), p.41

[11] D. Cheng and B. Li: Talanta. Vol. 78 (2009), p.949

[12] L. Zhao and H. K. Lee: Anal. Chem. Vol. 74 (2002), p.2486

[13] Z. Zhang, K. Zhou, Y. Q. Bu, Z. J. Shan, J. F. Liu, X. Y. Wu, L. Q. Yang and Z. L. Chen: Anal. Methods. Vol. 4 (2012), p.429

[14] E. Aguilera-Herrador, R. Lucena, S. Cardenas and M. Valcarcel: TrAC, Trends Anal. Chem. Vol. 29 (2009), p.602

[15] S. Dadfarnia and A. M. Haji Shabani: Anal. Chim. Acta. Vol. 658 (2010), p.107

[16] M. Ramos Payan, M. A. Bello Lopez, R. Fernandez-Torres, M. Callejon Mochon and J. L. Gomez Ariza: Talanta. Vol. 82 (2010), p.854

[17] M. Ramos Payan, M. A. Bello Lopez, R. Fernandez-Torres, J. A. Gonzalez and M. Callejon Mochon: J. Pharm. Biomed Anal. Vol. 55 (2011), p.332

[18] J. F. Liu, J. F. Peng, Y. G. Chi and G. B. Jiang: Talanta. Vol. 65 (2005), p.705

[19] J. F. Liu, Y. G. Chi and G. B. Jiang: J. Sep. Sci. Vol. 28 (2005), p.87

[20] J. Jing, X. L. Shao, Z. Chang, X. Y. Wu and Z. Zhang: Chinese J. Anal. Chem. Vol. 40 (2012), p.1257

[21] Y. Tao, J. F. Liu, X. L. Hu, H. C. Li, T. Wang and G. B. Jiang: J. Chromatogr. A. Vol. 1216 (2009), p.6259

[22] Y. Tao, J. F. Liu, T. Wang and G. B. Jiang: J. Chromatogr. A. Vol. 1216 (2009), p.756

[23] L. H. Yang, T. G. Luan and C. Y. Lan: J. Chromatogr. A. Vol. 1104 (2006), p.23

[24] J. F. Peng, J. F. Liu, X. L. Hu and G. B. Jiang: J. Chromatogr. A. Vol. 1139 (2007), p.165

[25] M. Mirzaei and H. Dinpanah: J. Chromatogr. B Analyt. Technol. Biomed Life Sci. Vol. 879 (2011), p.1870

[26] C. Desoubries, F. Chapuis-Hugon, A. Bossee and V. Pichon: J. Chromatogr. B Analyt. Technol. Biomed Life Sci. Vol. 900 (2012), p.48

[27] L. Zhu, K. H. Ee, L. Zhao and H. K. Lee: J. Chromatogr. A. Vol. 963 (2002), p.335

[28] M. H. Ma and F. F. Cantwell: Anal. Chem. Vol. 71 (1999), p.388