A New Method Using Liquid Chromatography Tandem Mass Spectrometry to Detect NDMA in Water

Chao Jie Zhang; Geng Zhang; Lu Ting Chen; Qian Chen; Qi Zhou

doi:10.4028/www.scientific.net/AMR.742.355

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A New Method Using Liquid Chromatography Tandem Mass Spectrometry to Detect NDMA in Water
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HomeAdvanced Materials ResearchAdvanced Materials Research Vol. 742A New Method Using Liquid Chromatography Tandem...

A New Method Using Liquid Chromatography Tandem Mass Spectrometry to Detect NDMA in Water

Abstract:

This study focused on using liquid Chromatography Tandem Mass Spectrometry to detect N-Nitrosodimethylamine (NDMA) at trace concentrations in water. The water sample was preconcentrated by solid-phase extraction method. To find an elution which can obtain higher recovery, three reagents with different organic solvents were examined. After comparing the recoveries and the standard deviation of the elution, finally the dichloromethane was determined as the elution of the experiment. Then the concentrated sample was analyzed by a method combining SPE pretreatment and LC separation with tandem mass spectrometry using multiple reaction monitoring (MRM).

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Periodical:

Advanced Materials Research (Volume 742)

Pages:

355-358

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.742.355

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Online since:

August 2013

Authors:

Chao Jie Zhang, Geng Zhang, Lu Ting Chen, Qian Chen, Qi Zhou

Keywords:

Liquid Chromatography Mass Spectrometry, N-Nitrosodimethylamine, Solid-Phase Extraction (SPE)

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References

[1] P. Andrzejewski and J. Nawrocki: Global Nest Journal, Vol.7 (2005), No 1, pp.27-42

Google Scholar

[2] Yuan - yuan Zhao , Jessica Boyd ,Stevee Hrudey , and Xing- Fang Li: Environ. Sci. Technol. 40(2006), pp.7636-7641

Google Scholar

[3] Bin Xu , Cao Qin , Chen-Yan Hu , Yi-Li Lin , Sheng-Ji Xia , Qian Xu , Seleli Andrew Mwakagenda, Xiang-yu Bi and Nai-Yun Gao: Science of the Total Environment, Vol. 417 (2012) pp.241-247

DOI: 10.1016/j.scitotenv.2011.12.056

Google Scholar

[4] Jean W. Munch and Margarita V. Bassett: Journal of Aoac international VOL. 89(2006), No. 2, p.487

Google Scholar