SnO2 Nanoparticle Synthesized by Ultrasonic-Assisted Process

Russameeruk Noonuruk; Wanichaya Mekprasart; Narongdet Wongpisutpaisan; Naratip Vittayakorn; Wisanu Pecharapa

doi:10.4028/www.scientific.net/AMR.770.299

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HomeAdvanced Materials ResearchAdvanced Materials Research Vol. 770SnO2 Nanoparticle Synthesized by...

SnO₂ Nanoparticle Synthesized by Ultrasonic-Assisted Process

Abstract:

SnO₂ nanoparticles were synthesized by ultrasonic-assisted precipitation process using stannic chloride pentahydrate (SnCl₄·5H₂O) as a precursor. The stannic chloride aqueous solution was precipitated by ammonia under sonication. The as-synthesized precipitates were dried at 80 oC and then calcined at 400 oC for 2 h. The physical properties of nanoparticles with/without sonication were characterized by thermogravimetic and differential thermal analysis, X-ray diffraction, and transmission electron microscope. The results reveal that ultrasonic radiation has significant influence on phase transformation mechanism from Sn (OH)₄ to SnO₂, grain size and uniformity of SnO₂ nanoparticles.

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Periodical:

Advanced Materials Research (Volume 770)

Pages:

299-302

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.770.299

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Online since:

September 2013

Authors:

Russameeruk Noonuruk, Wanichaya Mekprasart, Narongdet Wongpisutpaisan, Naratip Vittayakorn, Wisanu Pecharapa

Keywords:

Precipitation, SnO₂Nanoparticles, Ultrasonic-Assisted

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