Determination of Hemp Crystallinity by Different Evaluation Method

Article Preview

Abstract:

This paper used X-ray diffraction, infrared spectroscopy and nuclear magnetic resonance (NMR) to determine the crystallinity of hemp fiber. The results show that the order of crystallinity is Segal method > Peak deconvolution method > Newman method > Infrared spectroscopy method. Both empirical formula and peak deconvolution method lead to deviation of crystallinity value. However, there is a less inaccuracy in peak deconvolution than empirical formula and could get detailed crystal parameters. Therefore, peak deconvolution method is more suitable than empirical formula for determination of crystallinity of hemp fiber.

You might also be interested in these eBooks

Info:

Periodical:

Advanced Materials Research (Volumes 781-784)

Pages:

2730-2733

Citation:

Online since:

September 2013

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2013 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

* - Corresponding Author

[1] L. Segal, J. J. Creely andA. E. Mattin: Text Res J. 29, 1959, p.786.

Google Scholar

[2] M. L. Nelson, R. T. O'Connor: J Appl Poly Sci. 8(14), 1964, pp.1325-1341.

Google Scholar

[3] R. H. Newman: Holzforschung. 58(1), 2004, pp.91-96.

Google Scholar

[4] R. H. Newman: Solid State Nuclear Magnetic Resonance. 15(1), 1999, pp.21-29.

Google Scholar

[5] R. H. Newman, J. AHemmingson: Holzforschung. 44(5), 1990, pp.351-356.

Google Scholar

[6] A. M Hindeleh, D. J Johnson: JPhysD: ApplPhys. 4(2), 1971, pp.259-263.

Google Scholar

[7] P. Sunkyu, J. O. Baker, M. E. Himmel, P. A. Parilla, D. K. Johnson. Biotechnology for biofuels. 3, 2010, p.10.

Google Scholar