In Air Synthesis of Bi2S3 and PbS Microcrystals by Thermolysis of Single-Source Precursors

Zhen Ni Du; Yong Cai Zhang

doi:10.4028/www.scientific.net/AMR.79-82.1343

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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 79-82In Air Synthesis of Bi2S3 and PbS Microcrystals by...

In Air Synthesis of Bi₂S₃ and PbS Microcrystals by Thermolysis of Single-Source Precursors

Abstract:

Without the protection of inert gases or vacuum environment, rod-like Bi2S3 and cubic-shaped PbS microcrystals were synthesized directly via pyrolyzing corresponding metal diethyldithiocarbamates in air at 300 °C for 3 h. The products have been characterized by X-ray diffraction and scanning electron microscope, and their possible formation mechanisms were also tentatively proposed. Furthermore, control experiments with multiple-source precursors revealed that our single-source precursors played an important role in preparing phase-pure Bi2S3 and PbS.

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Periodical:

Advanced Materials Research (Volumes 79-82)

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1343-1346

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.79-82.1343

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Online since:

August 2009

Authors:

Zhen Ni Du, Yong Cai Zhang

Keywords:

Chemical Synthesis, Crystal Growth, Semiconductor, Single-Source Precursors

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References

[1] C. Wu, J.B. Shi, C.J. Chen and J.Y. Lin: Mater. Lett. Vol. 60 (2006), p.3618.

Google Scholar

[2] A.U. Ubale, A.S. Daryapurkar and R.B. Mankar: Mater. Chem. Phys. Vol. 110 (2008), p.180.

Google Scholar

[3] P.W. Shen and J.T. Wang: Dictionary of Compounds (Shanghai Lexicographical Publishing House, Shanghai, 2002).

Google Scholar

[4] D. Fan, M. Afzaal and P. O'Brien: Coord. Chem. Rev. Vol. 251 (2007), p.1878.

Google Scholar

[5] A.C.C. Esteves and T. Trindade: Curr. Opin. Solid State Mater. Sci. Vol. 6 (2002), p.347.

Google Scholar

[6] Y.C. Zhang, W.W. Chen and X.Y. Hu: Mater. Lett. Vol. 61 (2007), p.4847.

Google Scholar

[7] Y.C. Zhang, T. Qiao and X.Y. Hu: J. Cryst. Growth Vol. 277 (2005), p.518.

Google Scholar

[8] G. Xie, Z.P. Qiao and M.H. Zeng: Cryst. Growth Des. Vol. 4 (2004), p.513.

Google Scholar

[9] X.P. Shen, G. Yin, W.L. Zhang and Z. Xu: Solid State Commun. Vol. 140 (2006), p.116.

Google Scholar

[10] A.F. Wells: Structural Inorganic Chemistry, fifth ed. (Oxford University Press, New York 1984).

Google Scholar

[11] S.V. Khare, S. Kodambaka and D.D. Johnson: Surf. Sci. Vol. 522 (2003), p.75.

Google Scholar