The Effect of Time Ageing of Spray-Deposited on the Growth of CdSe Nanoparticles

Abstract:

Cadmium Selenide (CdSe) was obtained by using spray-deposited method which is using the sodium selenosulfite as Se precursor and cadmium chloride (CdCI) as cadmium (Cd) precursor. Time for each spray-deposited was used as the main parameter to investigate the properties of CdSe nanoparticles. By using FESEM for surface morphology and X-ray Diffraction (XRD) studies reveal that the CdSe nanoparticles with cubic crystal structures. In this research, the effect of time of spray deposited was main parameter to know the CdSe properties. The set of time was set from 10 min until 50 min. From FESEM result the size of CdSe nanoparticles were in the range 60-70 nm and the crystalline was hexagonal from XRD result. By using Scherrer equation, the size of crystalline of CdSe nanoparticles was determined from XRD characterization, the size was 60-70 nm. The size of CdSe nanoparticles from FESEM images were 60-80nm.

• Periodical: Advanced Materials Research (Volume 832)
• Pages: 827-831
• DOI: https://doi.org/10.4028/www.scientific.net/AMR.832.827
• Online since: November 2013
• Authors: C.H. Rosmani, A.Z. Zainurul, Mohamad Rusop, S. Abdullah
• Keywords: Cadmium (Cd), FESEM, Nanoparticle, Selenide, X-Ray Diffraction (XRD)

References

[1] Shalini Singh,M. C. Rath, A.K. Singh, and T. Mukherjee, CdSe nanoparticles grown via radiolytic methods in aqueous solutions, Radiation Physics and Chemistry 80 (2001) 736-741

DOI: 10.1016/j.radphyschem.2011.01.015

[2] Shutang Shen, Xiaoling Zhang and Qiuhua Zhang. Trioctylphosphine as Both Solvent and Stabilizer to Synthesize CdS Nanorods Nanoscale Res Lett 4(2009) 1159-1165.

DOI: 10.1007/s11671-009-9375-x

[3] Sanh Hyuk In, Yong Hui Lee and Sang II Seok. Photoelectrochemical solar cells fabricated from porous CdSe and CdS layers Electrochimica Acta 55 (2010) 5665-5669.

DOI: 10.1016/j.electacta.2010.04.106

[4] Lan Wang, Xiudong Sun, Wenjing Liu and Bingyi Liu.High quality zinc-blende CdSe nanocrystals synthesized in a hexadecylamine–oleic acid–paraffin liquid mixture Materials Chemistry and Physics 120(2010) 54-60.

DOI: 10.1016/j.matchemphys.2009.10.020

[5] Jing Wang and Heyou Han. Hydrothermal synthesis of high-quality type-II CdTe/CdSe quantum dots with near-infrared fluorescence J Colloid Interface Sci 351(2010) 83-7.

DOI: 10.1016/j.jcis.2010.07.025

[6] P. Nemec, D.Mikes, J. Rohovec, E. Uhlirova, F. Trajonek and P. Maly. Light-controlled growth of CdSe nanocrystalline films prepared by chemical deposition Material Science B69- 70( 2000) 500-504.

DOI: 10.1016/s0921-5107(99)00284-6

[7] Yuyi Araki, Koji Ohkuno, Takeshi Furukawa and Junji Saraie. Green light emitting diodes with CdSe quantum dots. 301-302 (2007) 809-811.

DOI: 10.1016/j.jcrysgro.2006.11.105

[8] Zhou, X., et al., Photoluminescence of CdSe and CdSe/CdO·nH2O core/shell nanoparticles prepared in aqueous solution Optical Materials 29(2007) 1048-1054.

DOI: 10.1016/j.optmat.2006.04.003

[9] Takeshi Ota, et al., Micro-photoluminescence from CdSe quantum dots Journal of Crystal Growth 214/215 (2000) 778-781.

DOI: 10.1016/s0022-0248(00)00228-1

[10] Mi, Wen, Tian, Jintao, Weiguo and Xiaoyun, Temperature dependent synthesis and optical properties of CdSe quantum dots Ceramics International Ceramics International 38 (2012) 5575-5583

DOI: 10.1016/j.ceramint.2012.03.077

[11] Yordanov, G.G., H. Yoshimura, and C.D. Dushkin, Fine control of the growth and optical properties of CdSe quantum dots by varying the amount of stearic acid in a liquid paraffin matrix Colloids and Surfaces A: Physicochemical and Engineering Aspects 322(2008) 177-182.

DOI: 10.1016/j.colsurfa.2008.03.002

[12] Sharma, S.N., et al.,Ligand-dependent transient absorption studies of hybrid polymer:CdSequantum dot composites Solar Energy Materials and Solar Cells 100 (2012) 6-15.

DOI: 10.1016/j.solmat.2011.10.020

[13] Neeleshwar, S.Chen, C.Tsai, C.Chen, Y. Shyu, and S. Seehra, Size-dependent properties of CdSe quantum dots Physical Review B 71 (2005) 2012071-4 14] Liao, Y.-f. And W.-j. Li,Synthesis of CdSe quantum dots via paraffin liquid and oleic acid Journal of Zhejiang University SCIENCE A 9(2007) 133-136.

DOI: 10.1103/physrevb.71.201307

[15] Sun, M., et al., Shape evolution of CdSe nanocrystals in vegetable oils: A synergistic effect of selenium precursor Colloids and Surfaces A: Physicochemical and Engineering Aspects 350(2006) 91-100.

DOI: 10.1016/j.colsurfa.2009.09.010

[16] Yang, D., Q. Chen, and S. Xu, Synthesis of CdSe/CdS with a simple non-TOP-based route Journal of Luminescence 126(2007) 853-858.

DOI: 10.1016/j.jlumin.2006.12.010

[17] G.Yordanov, G., C. D.Dushkin, and E. Adachi, Early time ripening during the growth of CdSe nanocrytals in liquid paraffin Colloids and Surfaces A: Physicochem. Eng. Aspects 316 (2008) 37-45.

DOI: 10.1016/j.colsurfa.2007.08.014

[18] A. A Yang, M. A Barote and E. U Masumdar: Journal of Luminescence. 126 (2006) 853-858.

[19] Huibing Mao, Jing Chen, Jiqing Wang, Zhifeng Li, Ning Dai and Ziqiang Zhu: Physica E: Low-dimensional Systems and Nanostructures. 27(2005) 124-128.