Characterization and Gold Assaying Methods in the Assessment of Low Grade Gold Ore from Malaysia

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The low grade gold ore obtained from a local gold mine in Malaysia was characterized using X-ray fluorescence analysis and scanning electron microscope/ energy dispersive X-ray analysis for the deportment of gold. Acid digestion was carried out to determine iron, aluminium, sulphur and arsenic using ICP-OES. Chemical assaying methods viz aqua regia leaching and lead fire assay followed by acid digestion were conducted to determine the head grade of the gold ore. Assessment of gold using fire assay was found reliable to reduce the interferences from the gangue minerals. Despite the lower limit of detection of ICP-OES, there was no appreciable amount of gold detected in the samples leached using aqua regia because of the interference from the gangue minerals and also due to the interlocking of gold with aluminosilicates phase which require high pressure and temperature leaching using hydrofluoric acid to liberate the gold. ICP-OES analysis is reliable depending on the degree of liberation of gold during acid digestion. The head grade for this type of low grade gold ore was found to be in the range of 0.31 g/t to 0.55 g/t where the gold was highly associated with aluminosilicate minerals.

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243-247

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November 2013

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© 2014 Trans Tech Publications Ltd. All Rights Reserved

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[1] J.C., Van Loon and R.R., Barefoot, Determination of The Precious Metals: Selected Instrumental Methods, John Wiley & Sons, (1991).

DOI: 10.1180/minmag.1992.056.383.25

Google Scholar

[2] S.L., Chryssoulis, and J., McMullen, Chapter 2: Mineralogical investigation of gold ores, Developments in Mineral Processing, Vol. 15.

DOI: 10.1016/s0167-4528(05)15002-9

Google Scholar

[3] N., Geoffroy, and F., Cardarelli, Research Summary (Waste Decontamination): A Method for Leaching or Dissolving Gold from Ores or Precious Metal Scrap, Journal Of Metal, pp.47-50, (2005).

DOI: 10.1007/s11837-005-0168-0

Google Scholar

[4] M.R., Juvonen, A. Bartha, T.M., Lakomaa, L.A., Soikkeli, E., Bertalan, E.L., Kallio, and M., Ballok, Comparison of Recoveries by Lead Fire Assay and Nickel Sulfide Fire Assay in the Determination of Gold/ Platinum/ Palladium and Rhenium in Sulfide Ore Samples, Geostandards and Geoanalytical Research, 28 (1)(2004).

DOI: 10.1111/j.1751-908x.2004.tb01048.x

Google Scholar

[5] R.R., Barefoot, Review: Determination of the precious metals in geological materials by inductively coupled plasma spectrometry, Journal of Analytical Atomic Spectrometry, 13(1998)1077-1084.

DOI: 10.1039/a803216e

Google Scholar

[6] C.G., Anderson, Available: http: /www. campmontanatech. net/_Documents/ Published/Articles_Papers/fundamentals_of_the_analysis_of_gold_silver_and_platinum_group_metals. pdf. [Accessed: Oct, 2012].

Google Scholar

[7] J, Zhou, B, Jago And C, Martin, Establishing the Process Mineralogy Of Gold Ores, SGS Minerals Technical Bulletin, 2004-03.

Google Scholar

[8] K. M, Blyth, D.N., Phillips, and W-v., Bronswijk, Analysis of Gold Ores by Fire Assay, Journal of Chemical Education, 81(2004)1780-1782.

DOI: 10.1021/ed081p1780

Google Scholar

[9] G. S. Reddi, C. R. M. Rao, T. A. S. Rao, S. Vijaya Lakshmi, R. K. Prabhu, and T. R. Mahalingam, Nickel sulphide fire assay - ICPMS method for the determination of platinum group elements: a detailed study on the recovery and losses at different stages, Fresenius J Anal Chem (1994).

DOI: 10.1007/bf00323133

Google Scholar