Microwave Hydrothermal Synthesis of W-Doped CuS Nanoparticle

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Abstract:

The CuS nanoparticles precursor have been synthesized by microwave irradiation, using copper nitrate and thioacetamide (TAA) as raw materials, dodecyl sodium sulfate as surfactants. After the precursor had being split with n-butyl lithium for 14 days, we synthesized w-doped copper sulfide nanoparticles with microwave hydrothermal method. The samples were characterized by X-ray powder diffraction (XRD), scanning electron microscopy (SEM) and fluorescence spectra.

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196-199

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April 2014

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© 2014 Trans Tech Publications Ltd. All Rights Reserved

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[1] J Wang    B Chen,B Hou,    J Dong, Methods to prepare copper sulfide nano-particles.Chinese Journal of Inorganic Chemistry, 17(2001)275-278.

Google Scholar

[2] R V Kumar, O Palchik, Y Koltypin, et al. Sonochemical synthesis and characterization of Ag2S/PVA and CuS/PVA nanocomposite. Ultrason. Sonochem, 9 (2002) 65-70.

DOI: 10.1016/s1350-4177(01)00100-6

Google Scholar

[3] X Y Chen, Z H Wang, X Wang, et al. Synthesis of novel copper sulfide hollow spheres generated from copper(II)–thiourea complex. Journal of Crystal Growth, 263(2004) 570-574.

DOI: 10.1016/j.jcrysgro.2003.12.004

Google Scholar

[4] X H Liao, N Y Chen, S Xu, et al. A microwave assisted heating method for the preparation of copper sulfide nanorods. Journal of Crystal Growth, 252(2003) 593-598.

DOI: 10.1016/s0022-0248(03)01030-3

Google Scholar

[5] S Li, F Xu, Y Wang,  S Xu, L He, Preparation and characterization of CeO2 Nanopowders under microwave irradiation. Chinese Rare Earths, 28(2007)112-114.

Google Scholar

[6] H Cheng, B Cui, J Tian, P Yu, Z Chang, Preparation and characterization of Si-doped BaTiO3 nanosized powders and ceramics.Journal of Northwest University, 38(2008) 63-66.

Google Scholar

[7] Y Pu, S Ning , W Chen, S Chen, Effect of Dy2O3-doping on microstructure and properties of BaTiO3 ceramic.Journal of Xi'an Jiaotong University, 38 (2004)424-427.

Google Scholar

[8] G Li,Z Xu,W Chen,Q Nie, J Xia, Preparation of ternary metals disulfide nanotube.Chemical Journal of Chinese University, 24(2003)2155-2157.

Google Scholar