Preparation of 5-Sulfosalicylic Acid Modified Silica Gel and its Adsorption Performances for Lead

Article Preview

Abstract:

A new sorbent (SSA-SG) with 5-sulfosalicylic acid as functional group has been prepared and characterized with FTIR and then used as micro-column packing for enrichment of Pb (II). Enrichment conditions of lead were optimized. The enrichment factor reaches 200 and the dynamic sorption capacity was 15.46 mgg-1 for Pb (II). The proposed column enrichment procedure was applied for the preconcentration/separation and atomic absorption spectrometry (AAS) determination of Pb (II) in water samples successfully.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

864-867

Citation:

Online since:

June 2014

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2014 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

* - Corresponding Author

[1] M. Ezoddin, F. Shemirani, Kh. Abdi, M. K. Saghezchi, M.R. Jamali, Application of modified nano-alumina as a solid phase extraction sorbent for the preconcentration of Cd and Pb in water and herbal samples prior to flame atomic absorption spectrometry determination, Journal of Hazardous Materials 178 (2010).

DOI: 10.1016/j.jhazmat.2010.02.023

Google Scholar

[2] X.P. Huang, X.J. Chang, Q. He, Y.M. Cui, Y.H. Zhai, N. Jiang, Tris(2-aminoethyl) amine functionalized silica gel for solid-phase extraction and preconcentration of Cr(III), Cd(II) and Pb(II) from waters, Journal of Hazardous Materials 157 (2008 ) 154–160.

DOI: 10.1016/j.jhazmat.2007.12.113

Google Scholar

[3] M. Ghaedi, F. Ahmadi, Z. Tavakoli, M. Montazerozohori, A. Khanmohammadi, M. Soylak, Three modified activated carbons by different ligands for the solid phase extraction of copper and lead, J. Hazard. Mater. 152 (2008) 1248-1255.

DOI: 10.1016/j.jhazmat.2007.07.108

Google Scholar

[4] X.Z. Wu, P. Liu, Q.S. Pu, Q.Y. Sun, Z.X. Su, Preparation of dendrimer-like polyamidoamine immobilized silica gel and its application to online preconcentration and separation palladium prior to FAAS determination, Talanta 62 (2004) 918-923.

DOI: 10.1016/j.talanta.2003.10.011

Google Scholar

[5] Y.M. CUI, X.J. CHANG, X.B. ZHU, N. Jiang, Z. Hu, N. Lian, Nanometer SiO2 modified with 5~sulfosalicylic acid as selective solid~phase extractant for Fe (III) determination by ICP-AES from biological and natural water samples. Microchemical journal 86 (2007).

DOI: 10.1016/j.microc.2006.09.002

Google Scholar