Screen Printed Carbon Nano-Powder for Ascorbic Acid Determination with Differential Pulse Voltammetry

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Carbon nanopowder mixed with carbon ink was used as a working screen-printed electrode. This electrode consists of carbon nanopowder working electrode, carbon counter electrode, and silver/silver chloride reference electrode. The electrochemical behavior of ascorbic acid has been studied by cyclic voltammetry and differential pulse voltammetry with screen-printed carbon nanopowder electrode. The propose electrode will enhanced the sensitivity for antioxidance determination because increasing of the surface area of the working electrode. The voltammetric sensor offers several advantages to both the green chemistry and eco-friendly. The method was successfully employed with 2 microliter of the working solution dropped on the electrode surface. A linear concentration, limit of quantitation and limit of detection was sufficient for the ascorbic acid determination in the vitamin C tablet. The results obtained for the sample juices demonstrated that the powerful of the method.

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378-381

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June 2014

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© 2014 Trans Tech Publications Ltd. All Rights Reserved

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[1] B. Habibia, M.H. Pournaghi-Azar, Simultaneous determination of ascorbic acid, dopamine and uric acid by use of a MWCNT modified carbon-ceramic electrode and differential pulse voltammetry, Electrochim Acta 55 (2010) 5492–5498.

DOI: 10.1016/j.electacta.2010.04.052

Google Scholar

[2] W. Wonsawat, S. Chuanuwatanakul, W. Dungchai, E. Punrat, S. Motomizu, O. Chailapakul, Graphene-carbon paste electrode for cadmium and lead ion monitoring in a flow-based system, Talanta 100 (2012) 282–289.

DOI: 10.1016/j.talanta.2012.07.045

Google Scholar

[3] T. Kondo, H. Sakamoto,T. Kato, M. Horitani, I. Shitand, M. Itagaki, M. Yuasa, Screen-printed diamond electrode: A disposable sensitive electrochemical electrode, Electrochem Commun 13 (2011) 1546–1549.

DOI: 10.1016/j.elecom.2011.10.013

Google Scholar

[4] J.H. Chen, W.Z. Li, D.Z. Wang, S.X. Yang, J.G. Wen, Z.F. Ren, Electrochemical characterization of carbon nanotubes as electrode in electrochemical double-layer capacitors, Carbon, 40 (2002) 1193–1197.

DOI: 10.1016/s0008-6223(01)00266-4

Google Scholar

[5] W. Wonsawat, W. Dungchai, S. Motomizu, S. Chuanuwatanakul, O. Chailapakul, Highly sensitive determination of cadmium and lead using a low-cost electrochemical flow-through cell based on a carbon paste electrode, Anal Sci, 28 (2012) 141-145.

DOI: 10.2116/analsci.28.141

Google Scholar

[6] R. Zhang, S. Liu, L. Wang, G. Yang, Electroanalysis of ascorbic acid using poly (bromocresol purple) film modified glassy carbon electrode, Measurement 46 (2013) 1089–1093.

DOI: 10.1016/j.measurement.2012.11.007

Google Scholar