Synthesis of Sodium Carboxymethyl Cellulose Based on Pretreated Bamboo Shaving

Wei Qing Chen; Dong Ping Lou

doi:10.4028/www.scientific.net/AMR.997.169

Paper Titles

Synthesis of Ni(II)-imprinted Mesoporous Silica Adsorbents by Surface Imprinting Technology for Removal of Ni(II) from Aqueous Solution
p.146

Effect of Temperature on Activities of Cell Wall Enzymes of Kiwifruit during the Shelf Life
p.150

The Application and Synthesis of Dipolyethylene Glycol Maleate
p.154

Food Grade Bioplastic Based on Corn Starch with Banana Pseudostem Fibre/Bacterial Cellulose Hybrid Filler
p.158

Synthesis of Sodium Carboxymethyl Cellulose Based on Pretreated Bamboo Shaving
p.169

Application of Foam Separation Technology to Tea Saponin Extraction
p.173

Effects of Compound Probiotics on Growth Performance, Intestinal Microflora and Immune Function of Broilers
p.178

Influence of Synthesis Parameters on the Formation of SAPO-5 from Metakaolin
p.185

Synthesis of 4-Subsituted-9-(2-deoxy-β-D-ribosyl)-7H-pyrimido[4,5-b]indole
p.189

HomeAdvanced Materials ResearchAdvanced Materials Research Vol. 997Synthesis of Sodium Carboxymethyl Cellulose Based...

Synthesis of Sodium Carboxymethyl Cellulose Based on Pretreated Bamboo Shaving

Abstract:

Bamboo shaving is a by-product of bamboo industry, often be discarded or incinerated. In this work, sodium carboxymethyl cellulose (CMC) was prepared from pretreated bamboo shaving as raw material, while the main reaction conditions affecting product properties such as pretreated method, alkalization temperature and time, etherified temperature and time were studied. The results showed that the optimized pretreated conditions for bamboo cellulose were soaked in 15% NaOH at 1:8 (w/v) ratio of cellulose to solvent for 1 h at 95°C, The content of α-cellulose reach to 94.25%. The optimized reaction conditions for CMC synthesis were alkalified at 30°C for 70 min and etherified at 55°C for 90min; afterwards, temperature was kept at 70°C for 10min. Under these conditions, viscosity of 1% CMC aqueous solution was above 260 mPa·s, degree of substitution (DS)≥0.8, and content of chloride and moisture were less than 1.2 % and 10 % respectively.