Preparation and Characterization of Anisotropic Ammonium Titanium Phosphate Crystals via Hydrothermal Route

Yun Hua Li; Yun Han Ling; Xin De Bai

doi:10.4028/www.scientific.net/KEM.280-283.597

Paper Titles

Novel Process for Synthesizing Nano-Ceramics Powder: Mechanical & Thermal Activation Processing
p.581

Preparation of MgAl₂O₄ Nanopowder by Homogeneous Precipitation Method
p.587

Study of the Technology of Chemical Copper Plating on Al-CuO Agglomerated Powders
p.591

Nanostructured Surface Coating Layer of Calcium Carbonate Composite Particles
p.593

Preparation and Characterization of Anisotropic Ammonium Titanium Phosphate Crystals via Hydrothermal Route
p.597

Biomimetic Synthesis of CaCO₃ Particles with Specific Size and Morphology
p.601

Study on the Synthetic Process of Calcium Borate
p.605

Synthesis of BiFeO₃-PbTiO₃ Powders by Sol-Gel Auto-Combustion Process
p.609

Process for Non-Agglomerated Nanometer-Sized Barium Titanate Powders by Sol-Gel Auto-Igniting Synthesis
p.613

HomeKey Engineering MaterialsKey Engineering Materials Vols. 280-283Preparation and Characterization of Anisotropic...

Preparation and Characterization of Anisotropic Ammonium Titanium Phosphate Crystals via Hydrothermal Route

Abstract:

A series of ammonium titanium phosphate nanocrystals were prepared by hydrothermal synthesis method, and characterized by XRD, IR, XPS, SEM and DTA/TG. The results showed that themicrostructures of the materials could be rod- or sphere-like nanocrystals with aqueous pH values changing from 0 to 5, and could be flake like nanocrystals when a certainty of oxalic acid was added to the hydrothermal systems. The hydrothermal duration and temperature were not the main factors influencing the morphology of the products, but longer time and higher temperature would make the material more highly crystalline. The hydrothermal synthesizing mechanism on different experimental conditions was also discussed.

You might also be interested in these eBooks

View Preview

Info:

Periodical:

Key Engineering Materials (Volumes 280-283)

Pages:

597-600

DOI:

https://doi.org/10.4028/www.scientific.net/KEM.280-283.597

Citation:

Cite this paper

Online since:

February 2007

Authors:

Yun Hua Li, Yun Han Ling, Xin De Bai

Keywords:

Ammonium Titanium Phosphate, Characterization, Hydrothermal Synthesis

Export:

RIS, BibTeX

Price:

Permissions CCC:

Request Permissions

Permissions PLS:

Request Permissions

Сopyright:

Citation:

References

[1] Y.J. Li, Z. Huang, X.M. Sun, Z. X Deng and Y. D Li: Mater. Chem. Phys. Vol. 76 (2002), p.119.

Google Scholar

[2] X.M. Sun, X. Chen, Z.X. Deng and Y.D. Li: Mater: Chem. Phys. Vol. 78 (2002), p.99.

Google Scholar

[3] X.W. Lou and H.C. Zeng: Chem. Mater. Vol. 14 (2002), p.4781.

Google Scholar

[4] W. Xun and Y.D. Li: Chem. Eur. J. Vol. 9 (2003), p.5627.

Google Scholar

[5] Y.J. Ji, H. Zhang, X.Y. Ma, J. Xu and D.R. Yang: J. Phys.: Condens. Matter. Vol. 15 (2003), pp. L661.

Google Scholar

[6] S.H. Yu, B. Liu, M.S. Mo, X.M. Huang and Y.T. Qian: Adv. Funct. Mater. Vol. 13 (2003), p.639.

Google Scholar

[7] A. N. Christensen and E.K. Anderson, I.G. Anderson, G. Alberti, M. Nielsen and M. Lehmann: Acta Chemica Scandinavica. Vol. 44 (1990), p.865.

Google Scholar

[8] D.M. Poojary, A.I. Bortun, L. N. Bortun and A. Clearfield: Vol. 132 (1997), p.213.

Google Scholar

[9] M. Tieme and F. SchÜth: Microporous and Mesoporous Materials. Vol. 27 (1999), p.193.

Google Scholar

[10] Y. Berezski, M. Jaroniec, A.I. Bortun, D.M. Poojary and A. Clearfield: J Colloid and interface science. Vol. 191 (1997), p.442.

DOI: 10.1006/jcis.1997.4928

Google Scholar

[11] J.M. Dugald and R.M. Keith: J. Phys. Chem. Vol. 96 (1992), p.3458.

Google Scholar

[12] C. Z. Wu, D. wang, J. Yang and T.W. Li: J. Phys. Chem. B Vol. 107 (2003), p.13583.

Google Scholar