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Effect of Sintering Temperature on Structural, Electrical and Dielectric Parameters of Mn-Zn Nano Ferrites

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Abstract:

Mn-Zn ferrite powders (Mn0.5Zn0.5Fe2O4) were prepared by the chemical co-precipitation method. The effect of sintering temperature on the crystalline phase formation and dielectric properties were investigated by X-ray diffraction and impedance analyzer respectively. The TGA/DTA analysis was carried out to know decomposition mechanism. Ferrites decomposed to Fe3O4 above 873 K sintering temperature. Crystallite size increased with increasing sintering temperature between 7-13 nm. The resistivity decreased with increase in temperature showing semiconducting like behaviour. Activation energy was in the range of 0.70 to 0.77eV for these samples. Dielectric constant decreased with increasing frequency. Relaxation peak occurred for loss tangent versus frequency curves. The ac conductivity explained using small polaron tunnelling (SPT) model.

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Advanced Materials XII View Preview

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Periodical:

Key Engineering Materials (Volumes 510-511)

Pages:

163-170

DOI:

https://doi.org/10.4028/www.scientific.net/KEM.510-511.163

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Online since:

May 2012

Authors:

Humaira Anwar, Ashari Maqsood

Keywords:

AC Conductivity, Dielectric, Loss Tangent, Nanoparticle, X-Ray Techniques

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© 2012 Trans Tech Publications Ltd. All Rights Reserved

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