Mechanical Properties of La2O3-Al2O3 Ceramics Prepared by Microwave Sintering

Article Preview

Abstract:

The influence of La2O3 on the phase and microstructure evaluation and mechanical properties of La2O3-Al2O3 ceramics sintered with 2.45 GHz microwave energy was investigated. The results showed that La2O3 could densify the pure alumina with a lower sintering temperature and a short sintering time. La2O3 reacted with Al2O3 to form LaAl11O18 completely and the amount of LaAl11O18 increased with the increasing content of La2O3, distributing at the Al2O3 grain boundaries. The specimen doped with 10 vol.% and 15 vol.% La2O3 sintered at 1500 °C exhibited plenty of columnar grains with draw ratio about 1:4. The existence of columnar grains enhanced the microhardness and fracture toughness of La2O3-Al2O3 ceramics.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

265-268

Citation:

Online since:

July 2012

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2012 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

[1] W.H. Sutton, Microwave Processing of Ceramic Materials, Am. Ceram. Soc. Bull. 68 (1989) 376-386.

Google Scholar

[2] M.W. Porada, Microwave sintering of lead-based relaxor ferroelectric ceramics, MRS. Bull. 18 (1993) 51-57.

Google Scholar

[3] L.M. Sheppard, Microwave Sintering of Ce-Y-ZTA Composite, Am. Ceram. Soc. Bull. 67 (1988) 1656-1661.

Google Scholar

[4] J.D. Katz, R.D. Blake, Microwave sintering of multiple alumina composite components, Am. Ceram. Soc. Bull. 70 (1991) 1304-1307.

Google Scholar

[5] C. Herring, Effect of Change of Scale on Sintering Phenomena, J. Appl Phys. 21 (1950) 301-303.

Google Scholar

[6] W.H. Rhodes, Agglomerate and Particle Size Effects on SinteringYttria- Stabilized Zirconia, J. Am Ceram Soc. 64 (1981) 19-22.

Google Scholar

[7] F.F. Lange, Sinterability of Agglomerated Powders, J. Am Ceram Soc. 67 (1984) 86-89.

Google Scholar

[8] D.W. Readey, Mass Transport and Sintering of Impure Ionic Solids, J. Am Ceram Soc. 49 (1966) 366-369.

DOI: 10.1111/j.1151-2916.1966.tb13286.x

Google Scholar

[9] R.D. Bagley, I.B. Cutler, D.L. Johnson, Effect of TiO2 on Initial Sintering of Al2O3, J. Am Ceram Soc. 53 (1970) 136-141.

Google Scholar

[10] W.D. Kingery, Densification during Sintering in the Presence of a Liquid Phase, J. Appl Phys. 30 (1959) 301-306.

Google Scholar

[11] A.C. Anrunes, S.R. Pianaro, Effect of La2O3 doping on the microstructure and electrical properties of a SnO2-based varistor, J. Mater Sci. 36 (2001) 69-74.

Google Scholar