Eddy Current Characterization of (Fe65Co35)xAl1-x Nanocrystalline Alloy Synthesized by Mechanical Alloying Process

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An investigation was conducted to explore the applicability of Eddy Current (EC) and magnetic techniques to characterize the formation and grains size variation during Mechanical Alloying (MA) and the formation of a new mixture due to the variation of crystallography parameters. The change in apparent density was attributable to the irregular particles of the metal powders. A series of Nanocrystalline (Fe65Co35)xAl1-x samples have been prepared using M.A based on planetary ball mill under several milling conditions. M.A is a non-equilibrium process for materials synthesis. The structural effects of MA of powders were investigated by X-Ray diffraction analysis, SEM, microwaves, hysteresis magnetic and Eddy Current technique. Consequently, a nanostructure alloy was obtained with an average grain size of 8 nm. Experimental results show that fine nanocrystalline alloy powders prepared by mechanical milling are very promising for microwave applications and it is suggested that Eddy current measurement technique is a useful tool for the characterization of nanocrystalline materials.

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71-78

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April 2013

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© 2013 Trans Tech Publications Ltd. All Rights Reserved

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[1] E. Michael, 'Amorphous and nanocrystalline materials for applications as soft magnets', Progress in Materials Science 44 (1999) pp.291-433.

DOI: 10.1016/s0079-6425(99)00002-x

Google Scholar

[2] R. Bormann, 'Mechanical alloying fundamental mechanism and application', International Conference on Materials by Powder Technology, Dresden, Germany, (1993) p.247.

Google Scholar

[3] H. Moumeni, H., Alleg, S., Djebbari, C. and Bentayeb, F.Z. 'Synthesis and characterisation of nanostructured Fe-Co alloys', Journal of Material Science, Vol. 39, Nos. 16–17, (2004) p.5441.

DOI: 10.1023/b:jmsc.0000039262.37788.b7

Google Scholar

[4] T. Sourmail,' Near equiatomic FeCo alloys: Constitution, mechanical and magnetic properties', Progress in Materials Science 50 (2005) p.816–880.

DOI: 10.1016/j.pmatsci.2005.04.001

Google Scholar

[5] S. Varkey, N. Lakshmi, K. Venugopalan 'Correlation between microstructure and magnetic properties in mechanically alloyed nanogranular Fe100−xAlx Materials Letters' vol. 61, no23-24, (2007) pp.4635-4638.

DOI: 10.1016/j.matlet.2007.02.064

Google Scholar

[6] Q.Zeng. I. Baker, 'Magnetic properties and thermal ordering of mechanically alloyed Fe–40 at% Al', Intermetallics 14, (2006) p.396–405.

DOI: 10.1016/j.intermet.2005.07.005

Google Scholar

[7] A. Haddad, M. Zergoug, S. Bergheul, M. Azzaz, Monitoring of metal powder by eddy current, International journal of microstructure and materials properties,v5,n1,(2010)pp.3-14.

DOI: 10.1504/ijmmp.2010.032497

Google Scholar

[8] R.Grimberg, L.Udpa, A.Savin, R.Steigmann, V.Palihovici and Satish S. Udpa, 2D Eddy current sensor array, NDT & E International, V 39, Issue 4, (2006)pp.264-271.

DOI: 10.1016/j.ndteint.2005.08.004

Google Scholar

[9] S. Bergheul, A. Haddad, A.Tafat and M.Azzaz , 'Magnetic microwave and absorbing properties of Fe-Co alloy synthesised by mechanical alloying process', International journal of microstructure and materials properties,Vol. 1, 2006.

DOI: 10.1504/ijmmp.2006.011648

Google Scholar

[10] H. Moumeni, S. Alleg, and J.M. Greneche,'Structural properties of Fe-Co nanostructured powder prepared by mechanical alloying', Journal of Alloys and Compounds, Vol. 386,N. 1–2, (2005) p.12.

DOI: 10.1016/j.jallcom.2004.05.017

Google Scholar

[11] C.Djebbari, S.Alleg and J.M. Greneche. Effect of aluminum addition on the structural properties of nanostructured Fe50Co50 alloy, nuclear instruments and methods in physics research B, 268 (2010) pp.306-310.

DOI: 10.1016/j.nimb.2009.09.008

Google Scholar

[12] D. Prémel and A. Baussard,'Eddy-current evaluation of three-dimensional flaws in flat conductive materials using a Bayesian approach', Inverse Problems, V18, N6 ,2002.

DOI: 10.1088/0266-5611/18/6/326

Google Scholar