Microstructure and Local Mechanical Properties of Cu-Co Alloys after Severe Plastic Deformation

Article Preview

Abstract:

Microstructure of Cu-2wt.%Co alloy after various heat treatment (and hence with various phase constitution) was studied after equal-channel angular pressing (ECAP) using transmission electron microscopy (TEM) and electron backscatter diffraction (EBSD) technique in a scanning electron microscope (SEM). We also focused on local mechanical properties measured across the section perpendicular to the ECAP extrusion direction. Starting from the grain size well above 1mm in the Cu-2wt.%Co solid solution, ECAP subsequently reduces grain size down to the submicron level. A comparison with pure Cu shows that the grain size homogenization is shifted towards higher number of ECAP passes. Fine dispersion of precipitates further slows down the grain refinement and grain size homogenization during ECAP processing. Local mechanical properties measured across the section perpendicular to the ECAP extrusion direction reveal systematic inhomogeneities of deformed microstructure caused by local gradients of temperature and pressure and by the processing geometry itself. This should be considered while characterizing the microstructure by a single EBSD measurement on a small selected area.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

100-103

Citation:

Online since:

September 2013

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2014 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

[1] V.M. Segal, Materials processing by simple shear, Mater. Sci. Eng. A 197 (1995) 157-164.

Google Scholar

[2] R.Z. Valiev, R.K. Islamgaliev, I.V. Alexandrov, Bulk nanostructured materials from severe plastic deformation, Prog. Mater. Sci. 45 (2000) 103-189.

DOI: 10.1016/s0079-6425(99)00007-9

Google Scholar

[3] R.Z. Valiev, T.G. Langdon, Principles of equal-channel angular pressing as a processing tool for grain refinement, Prog. Mater. Sci. 51 (2006) 881-981.

DOI: 10.1016/j.pmatsci.2006.02.003

Google Scholar

[4] I. Saxl, V. Sklenička, L. Ilucová, M. Svoboda, P. Král, J. Dvořák, Characterization of creep behaviour and microstructure changes in pure Cu processed by ECAP, Rev. Adv. Mater. Sci. 25 (2010) 233-240.

DOI: 10.4028/www.scientific.net/msf.503-504.245

Google Scholar

[5] J. Buršík, P. Král, J. Dvořák, M. Svoboda, V. Sklenička, Microstructure of Cu-Co alloy after severe plastic deformation studied by EBSD, Proceedings of European Microscopy Congress, Manchester, 2012, PS1. 4.

DOI: 10.4028/www.scientific.net/kem.586.100

Google Scholar

[6] J. Buršík, M. Svoboda, P. Král, J. Dvořák, V. Sklenička, TEM and SEM study of precipitation hardened Cu-Co alloys after severe plastic deformation, NANOCON 2012, Conference Proceedings, Brno, 2012, p.86, full paper on CD.

DOI: 10.4028/www.scientific.net/kem.592-593.720

Google Scholar

[7] K.L. Johnson, The correlation of indentation experiments, J. Mech. Phys. Solids 18 (1970) 115-126.

Google Scholar

[8] W.C. Oliver, G.M. Pharr, Measurement of hardness and elastic modulus by instrumented indentation: advances in understanding and refinements to methodology, J. Mater. Res. 19 (2004) 3-20.

DOI: 10.1557/jmr.2004.19.1.3

Google Scholar