Effect of Temperature on Structural and Optical Properties of ZnO Nanorods by Hydrothermal Method

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The ZnO nanorods were prepared at 130 °C, 160 °C and 190 °C for 6 h by hydrothermal method. The structural and optical properties of ZnO nanorods were invesitigated by powder X-ray diffraction (PXRD), scanning electron microscopy (SEM) and Fourier transform infrared spectroscopy (FTIR). XRD pattern analysis showed that the ZnO nanorods are the hexagonal structure (space group P63 mc). No other crystal phases, such as Zn and Zn (OH)2 were detected. FT-IR study identified the sharp peak that appeared at 573 cm-1 is related with the ZnO stretching mode. Also, SEM images revealed that the diameter of a single ZnO crystal ranges from 100 to 300 nm and the length ranges from 1 to 3 μm.

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293-296

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November 2013

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© 2014 Trans Tech Publications Ltd. All Rights Reserved

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[1] H. Ohta, K.I. Kawamura, M. Orita, Current injection emissionfrom a transparent p–n junction composed of p-SrCu2O2/n-ZnO, Appl. Phys. Lett. 77(2000) 475–477.

DOI: 10.1063/1.127015

Google Scholar

[2] M.S. Arnold, P. Avouris, Z.W. Pan, Field-effect transistors based on single semiconducting oxide nanobelts, J. Phys. Chem. B. 107 (2003) 659–663.

DOI: 10.1021/jp0271054

Google Scholar

[3] J.Y. Lee, Y.S. Choi, J.H. Kim, Optimizing n-ZnO/p-Si heterojunctions for photodiode applications, Thin Solid Films. 403 (2002) 553–557.

DOI: 10.1016/s0040-6090(01)01550-4

Google Scholar

[4] Z. Pan, Z.L. Wang, E. Comini, Stable and highly sensitive gas sensors based on semiconducting oxide nanobelts, Appl. Phys. Lett. 81 (2002) 1869–1871.

DOI: 10.1063/1.1504867

Google Scholar

[5] J. Xu, Y. Chen, D. Chen, Hydrothermal synthesis and gas sensing characters of ZnO nanorods, Sens. Actuators. B. 113 (2006) 526–531.

DOI: 10.1016/j.snb.2005.03.097

Google Scholar

[6] Y. Chen, R. Yu, Q. Shi, Hydrothermal synthesis of hexagonal ZnO clusters, Mater. Lett. 61 (2007) 4438–4441.

DOI: 10.1016/j.matlet.2007.02.028

Google Scholar

[7] C.L. Jiang, W.Q. Zhang, G.F. Zou, Hexagonal and prismatic nanowalled ZnO microboxes, J. Phys. Chem. B. 109 (2005) 1361–1363.

DOI: 10.1021/ic051833z.s001

Google Scholar

[8] Y. Wang., X. Li, G. Lu, Synthesis and photo-catalytic degradation property of nanostructured-ZnO with different morphology, Mater. Lett. 62 (2008) 2359–2362.

DOI: 10.1016/j.matlet.2007.12.019

Google Scholar

[9] L. Wu, Y. Wu, W. Lu, Preparation of ZnO Nanorods and optical characterizations, Physica. E. 28 (2005) 76–82.

Google Scholar

[10] S. Anas, R.V. Mangalaraja, S. Ananthakumar, Studies on the evolution of ZnO morphologiesin a thermohydrolysis technique and evaluation of their functional properties, J. Hazard. Mater. 175(2010) 889–895.

DOI: 10.1016/j.jhazmat.2009.10.093

Google Scholar