Synthesis of Nanopowders of Magnesium Diboride by Magnesium Thermic Reduction under the Conditions of High Pressure of Argon

Amanbol Alipbaev; Sergey Fomenko; Zulkhair Mansurov; Roza Abdulkarimova; Vladimir Zarko

doi:10.4028/www.scientific.net/KEM.733.56

Paper Titles

An Experimental Analysis of Lactic Acid Esterification Process Using Langmuir-Hinshelwood Model
p.36

Separation of Methane from Shuttle Tanker Vents Gases by Adsorption on a Polyurethane/Zeolite Membrane
p.42

Neutronic Analysis of Thorium Nitride (Th, U233)N Fuel for 500MWth Gas Cooled Fast Reactor (GFR) Long Life without Refueling
p.47

Combined Method for the Synthesis of Ultrafine Powder Carbides of W, Ti, V
p.51

Synthesis of Nanopowders of Magnesium Diboride by Magnesium Thermic Reduction under the Conditions of High Pressure of Argon
p.56

Water Absorption, Friction and Wear Behaviors of Polypropylene Composites Filled with Hydroxyapatite
p.60

Effects of Olive Pit and Almond Shell Powder on Polypropylene
p.65

Effect of Nanotechnology on Physical Properties of Concrete
p.71

Effect of Plasticizers and Water on Properties of HCFA Geopolymers
p.76

HomeKey Engineering MaterialsKey Engineering Materials Vol. 733Synthesis of Nanopowders of Magnesium Diboride by...

Synthesis of Nanopowders of Magnesium Diboride by Magnesium Thermic Reduction under the Conditions of High Pressure of Argon

Abstract:

Magnesium diboride obtained from magnesium and boron oxide by magnesium-thermal reduction in SHS mode under the high-pressure inert gas (argon) was investigated. The effect of pressure of inert gas on the temperature of synthesis and the yield of final product (magnesium diboride) was determined. As energy additives were used powerful oxidizers - potassium chlorate salt (KClO₃) and ammonium nitrate (KNO₃) to increase the reactivity of the system Mg - B₂O₃. The composite material containing up to 20% of magnesium diboride phase was obtained. The acidic separation of final product from impurities was suggested. The microstructure and characteristic of particle size was defined. The products had a dense grain structure with a particle size 200-500 nm.

You might also be interested in these eBooks

Materials and Technologies in Modern Industrial Production

View Preview

Info:

Periodical:

Key Engineering Materials (Volume 733)

Pages:

56-59

DOI:

https://doi.org/10.4028/www.scientific.net/KEM.733.56

Citation:

Cite this paper

Online since:

March 2017

Authors:

Amanbol Alipbaev, Sergey Fomenko, Zulkhair Mansurov, Roza Abdulkarimova, Vladimir Zarko

Keywords:

Boron Oxide, Magnesium Diboride, Self-Propagating High Temperature Synthesis

Export:

RIS, BibTeX

Price:

Permissions CCC:

Request Permissions

Permissions PLS:

Request Permissions

Сopyright:

Citation:

References

[1] Ivanovskii A.L., Superconductor MgB2 and related compounds synthesis, properties, electron structure/ A.L. Ivanovskii / Successes of chemistry -70. —2001. — P. 811- 829.

Google Scholar

[2] Larbalestier D. C., Cooley L. D., et al. Strongly linked current flow in polycrystalline forms of the superconductor MgB2 / Nature. — 2001. — V. 410. — P. 186–189.

DOI: 10.1002/chin.200125013

Google Scholar

[3] Przybylski K., Stobierski L., Chmist J., Ko_lodziejczyk A. Synthesis and properties of MgB2 obtained by SHS method / Physica C. — 2003. — V. 387. — P. 148–152.

DOI: 10.1016/s0921-4534(03)00661-0

Google Scholar

[4] Rosenband V., Gany A., Synthesis of magnesium diboride powder under the conditions of thermal explosion/ Comb., Explo., and Shock Waves. — 2014. — V. 50, No. 6. — P. 34-39.

DOI: 10.1134/s0010508214060057

Google Scholar

[5] Nagamatsu J., Nakagawa N., Muranaka T., Zenitani Y., Akimitsu J. nature 410, 410, 63(2001).

DOI: 10.1038/35065039

Google Scholar

[6] Zlotnikov I., Gotman I., Gutmanas E. Y. Processing of dense bulk MgB2 superconductor via pressure-assisted thermal explosion mode of SHS / J. Europ. Ceram. Soc. —2005. —V. 25. — P. 3517–3522.

DOI: 10.1016/j.jeurceramsoc.2004.09.009

Google Scholar

[7] Perminov V.P., Magnesium-thermic off-furnace production of boron from boric anhydride/ powder metallurgy, 1998 № 2, P. 1.

Google Scholar