Effect of Cooling Rate on the Microstructural and Mechanical Properties of Sn-0.3Ag-0.7Cu-0.05Ni Solder Alloy

Article Preview

Abstract:

The effect of cooling rate on the microstructural and mechanical properties of Sn-0.3Ag-0.7Cu-0.05Ni lead-free solder alloy was studied. The microstructure of specimens was characterized by using an optical microscope (OM) and an energy dispersive X-ray spectroscopy (EDX). The mechanical properties were performed by using a universal testing machine (UTM). The results showed that the cooling rate of water-cooled specimens was about 2.37 °C/s and the cooling rate of mold-cooled specimens was about 0.05 °C/s. To compare the different cooling rates, it was found that the grain size of water-cooled specimens was finer than that of the mold-cooled specimens, this resulted in an increment of mechanical properties of solder alloy. A higher tensile strength (33.10 MPa) and a higher elongation (34%) were observed when water-cooled and mold-cooled systems were used, respectively. The microstructure of Sn-0.3Ag-0.7Cu-0.05Ni lead-free solder alloy solidified by both cooling systems exhibited three phases: β-Sn, Ag3Sn and (Cu,Ni)6Sn5 IMCs.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

9-13

Citation:

Online since:

August 2017

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2017 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

* - Corresponding Author

[1] H. Choi, T.K. Lee, Y. Kim, H. Kwon, C.F. Tseng, J.G. Duh, H. Choe, Improved strength of boron-doped Sn–1. 0Ag–0. 5Cu solder joints under aging conditions, Intermetallics 20(1) (2012) 155-159.

DOI: 10.1016/j.intermet.2011.09.008

Google Scholar

[2] A. Fawzy, S.A. Fayek, M. Sobhy, E. Nassr, M.M. Mousa, G. Saad, Tensile creep characteristics of Sn-3. 5Ag-0. 5Cu (SAC355) solder reinforced with nano-metric ZnO particles, Mater. Sci. Eng. A 603 (2014) 1-10.

DOI: 10.1016/j.msea.2014.02.061

Google Scholar

[3] K. Kanlayasiri, T. Ariga, Influence of thermal aging on microhardness and microstructure of Sn-0. 3Ag-0. 7Cu-xIn lead-free solders, J. Alloy Compd. 504 (2010) L5-L9.

DOI: 10.1016/j.jallcom.2010.05.057

Google Scholar

[4] A.A. El-Daly, A.E. Hammad, A. Fawzy, D.A. Nasrallh, Microstructure, mechanical properties, and deformation behaviour of Sn-1. 0Ag-0. 5Cu solder after Ni and Sb additions, Mater. Design 43 (2013) 40-49.

DOI: 10.1016/j.matdes.2012.06.058

Google Scholar

[5] Microstructural modifications and properties of low-Ag-content Sn-Ag-Cu solder joints induced by Zn alloying, J. Alloy Compd. 653 (2015) 402-410.

DOI: 10.1016/j.jallcom.2015.09.033

Google Scholar

[6] K. Mehrabi, F. khodabakhshi, E. Zareh, A. Shahbazkhan, A, Simchi, Effect of alumina nanoparticles on the microstructure and mechanical durability of meltspun lead-free solders based on tin alloys, J. Alloy Compd. 688 (2016) 143-155.

DOI: 10.1016/j.jallcom.2016.06.296

Google Scholar

[7] K.S. Kim, S.H. Huh, K. Suganuma, Effects of cooling speed on the microstructure and tensile properties of Sn-Ag-Cu alloys, Mater. Sci. Eng. A 333 (2002) 106-114.

DOI: 10.1016/s0921-5093(01)01828-7

Google Scholar

[8] L.R. Garcia, W.R. Osorio, A. Garcia, The effect of cooling rate on the dendritic spacing and morphology of Ag3Sn intermetallic particles of a SnAg solder alloy, Mater. Design 32 (2011) 3008-3012.

DOI: 10.1016/j.matdes.2010.12.046

Google Scholar

[9] S.K. Seo, S.K. Kang, D.Y. Shih, H.M. Lee, An investigation of microstructure and microhardness of Sn-Cu and Sn-Ag solders as functions of alloy composition and cooling rate J. Elec. Mater. 38 (2009) 257-265.

DOI: 10.1007/s11664-008-0545-x

Google Scholar

[10] R. Li, R. Xin, Q. Liu, A. Chapuis, S. Liu, G. Fu, L. Zong, Effect of grain size, texture and density of precipitates on the hardness and tensile yield stress of Mg-14Gd-0. 5Zr alloys, Mater. Design 114 (2017) 450–458.

DOI: 10.1016/j.matdes.2016.10.074

Google Scholar

[11] A.A. El-Daly, A.M. El-Taher, Improved strength of Ni and Zn-doped Sn-2. 0Ag-0. 5Cu lead-free solder alloys under controlled processing parameters, Mater. Design 47 (2013) 607-614.

DOI: 10.1016/j.matdes.2012.12.081

Google Scholar

[12] A.E. Hammad, Evolution of microstructure, thermal and creep properties of Ni-doped Sn-0. 5Ag-0. 7Cu low-Ag solder alloys for electronic applications, Mater. Design 52 (2013) 663-670.

DOI: 10.1016/j.matdes.2013.05.102

Google Scholar