SEM Analysis of the Interface of Five Adhesive Systems

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The aim of this study was to investigate the interface ultrastructure at dentin and hybrid layer formed by novel adhesives with TiO2 nano-fillers. Nano-fillers have shown outstanding mechanical properties and they are widely used as reinforcing materials associated with polymeric matrices for high performance applications. Twenty extracted non carious human teeth were utilized for evaluation of the bonded interface using scanning electron microscopy. The experiments used four novel adhesives (noted A1, A2, A3, A4). Phosphoric acid (5s, 37%) and a commercial resin composite Herculite XRV (Kerr) filling were used for the surface treatment. The interface was studies using scanning electron microscopy (SEM) using a microscope Inspect F-FEI Company. The experimental results indicated the main benefits and disadvantages of the investigated adhesives systems. SEM of the adhesive dentin interface revealed a HAp (hydroxyapatite) – rich and homogenous hybrid layer. This layer produced a favourable sealing of damaged dentin.

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18-23

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August 2017

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© 2017 Trans Tech Publications Ltd. All Rights Reserved

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[1] N. Nakabayashi, M. Nakamura, N. Yasuda, Hybrid layer as a dentin-bonding mechanism. J. Aesthetic Rest. Dent. 3 (1991) 133-138.

DOI: 10.1111/j.1708-8240.1991.tb00985.x

Google Scholar

[2] H. Sano, M. Yoshiyama, S. Ebisu, M.F. Burrow, T. Takatsu, B. Ciucchi, R. Carvalho, D.H. Pashley, Comparative SEM and TEM observation of nanoleakage within the hybrid layers, Oper. Dent. 20(4) (1995) 160-164.

Google Scholar

[3] J. Sun, E. J. Petersen, S. S. Watson, C. M. Sims, A. Kassman, S. Frukhtbeyn, D. Skrtic, M. T. Ok, D. S. Jacobs, V. Reipa, Q. Ye, B. C. Nelson, Biophysical characterization of functionalized titania nanoparticles and their application in dental adhesives, Acta Biomaterialia, 53 (2017).

DOI: 10.1016/j.actbio.2017.01.084

Google Scholar

[4] D. Prodan, A. Molea, M. Moldovan, V. Popescu, L. Silaghi-Dumitrescu, C. Prejmerean, S. Boboia, C. Sarosi, Synthesis and characterization of the hydroxyapatite and TiO2 doped hydroxyapatite powders, JOAM 16(11-12) (2014) 1300 - 1305.

DOI: 10.4028/www.scientific.net/kem.587.43

Google Scholar

[5] M.C. Cagidiaco, M. Ferrari, A. Vichi, Mapping of tubule and intertubule surface areas available for bonding in Class V and Class II preparations, J. Dent. 25 (1997) 379-389.

DOI: 10.1016/s0300-5712(96)00060-7

Google Scholar

[6] B. Haller, N. Hofmann, B. Klaiber, U. Bloching, Effect of storage media on microleakage of five dentin bonding agents, Dent Mater. 9(3) (1993) 191-197.

DOI: 10.1016/0109-5641(93)90119-b

Google Scholar

[7] A. Albaladejo, R. Osorio, M. Toledano, M. Ferrari, Hybrid layers of etch- and- rinse versus self-etching adhesive systems, Med. Oral. Patol. Oral. Cir. Bucal. 15(1) (2010) 112-118.

DOI: 10.4317/medoral.15.e112

Google Scholar

[8] S. Kenshima, C. Francci, A. Reis, A.D. Loguercio, L.E.R. Filho, Conditioning effect on dentin, resin tags and hybrid layer of different acidity self-etch adhesives applied to thick and thin smear layer, J. Dent. 34(10) (2006) 775-83.

DOI: 10.1016/j.jdent.2006.03.001

Google Scholar

[9] I. Watanabe, N. Nakabayashi, D.H. Pashley, Bonding to ground dentin by Phenyl-P self-etching primer, J. Dent. Res. 73 (1994) 1212-1220.

DOI: 10.1177/00220345940730061301

Google Scholar

[10] J.O.A.P. Cal-Neto, M.S. Miranda, K.R.H.C. Dias, Comparative SEM evaluation of penetration of adhesive systems in human dentin with a non rinse conditioner and a self-etching primer, Brazil. Dent. J. 15 (2004) 19-25.

DOI: 10.1590/s0103-64402004000100004

Google Scholar

[11] J. Kim, S. Mai, F.R. Tay, All in one adhesive does not etch beyond hybrid layers, J. Dent. Research. 89(5) (2010) 482-487.

DOI: 10.1177/0022034510363665

Google Scholar

[12] L. Tjaderhane, F.D. Nascimento, L. Breschi, A. Mazzoni, I.L.S. Tersariol, S. Geraldeli, A.T. Mutluay, M. Arrilho, R.M. Carvalho, F.R. Tay, D.H. Pashley, Strategies to prevent hydrolytic degradation of the hybrid layer-A review, Dent. Mat. 29 (10) (2013).

DOI: 10.1016/j.dental.2013.07.016

Google Scholar

[13] U. Lohbauer, S.A. Nikolaenko, A. Petschelt, R. Frankenberg, Resin tags do not contribute to dentin adhesion in self-etching adhesives, J. Adhesive Dent. 10 (2008) 97-103.

Google Scholar

[14] R.H. Sunfeld, C.H. Oliviera, A. Silva, A.L. Briso, M.L. Sundefeld, Resin tag length of one step and self etching adhesives bonded to unground enamel, Bull. Tokyo. Dent. Coll. 46(3) (2005) 43-49.

DOI: 10.2209/tdcpublication.46.43

Google Scholar

[15] E. Eliguzeloglu, H. Omurlu, G. Eskitascioglu, S. Belli, Effect of surface treatments and different adhesives on the hybrid layer thickness of on carious cervical lesions. Oper. Dent. 33(3) (2008) 338- 345.

DOI: 10.2341/07-96

Google Scholar