Synthesis of Brookite-Typed Titania from Titanium Chloride Solution

Satoshi Okano; Saeki Yamamuro; Toshiro Tanaka

doi:10.4028/www.scientific.net/MSF.610-613.285

Paper Titles

Effect of the Superfine SiO₂ Powder Content on the Properties of SiC Composites
p.262

Synthesis of O'-SiAlON/SiC Ecomaterials by Using Non-Traditional Resources: Yangtze River Sand
p.267

Investigation of the SCR Catalyst Ce-V/TiO₂
p.274

Preparation of Eco-Friendly Composite Ceramic from Iron Ore Tailings
p.281

Synthesis of Brookite-Typed Titania from Titanium Chloride Solution
p.285

Preparation and Characterization of TiO₂ Nanowires on Aluminum Substrate
p.288

Photo-Catalytic Activity of Cu₂O Films with Various Crystal Structures Prepared by DC Reactive Magnetron Sputtering
p.293

Influence of Silver / CNTs on Epoxide Resin Based Conductive Adhesive
p.299

Degradation of Harmful Gases in Air by Ce³⁺/TiO₂ Complex Nanomembrane
p.304

HomeMaterials Science ForumMaterials Science Forum Vols. 610-613Synthesis of Brookite-Typed Titania from Titanium...

Synthesis of Brookite-Typed Titania from Titanium Chloride Solution

Abstract:

The brookite-phase TiO2 was prepared by a hydrothermal synthesis of titanium chloride solution. The thermolysis time and the pH value of the solution were controlled during the synthesis. X-ray diffraction experiments showed that TiO2 powders partially containing the brookite-phase were successfully obtained. A higher amount of OH- in the reaction solution was found to be important to obtain the brookite phase because the intermediate complex leading to the brookite phase consumes more amount of OH- than other phases like the rutile.