Evolution of Intermetallic Phase Fe2(W, Mo) in 9% Cr Steel during Creep Rupture Tests at 650°C

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Abstract:

Our report deals with investigation of evolution of AB2 phase in three melts of new 9% Cr heat resistant steel with different chemical compositions during creep rupture tests at 650°C in the course of 10000 hours. For each sample the following research procedure was applied: (i) identification of all second phases precipitations using differential X-ray analysis method; (ii) study of spatial distribution of second phases using scanning electron microscope and transmission electron microscope; (iii) numerical investigation of mass fraction and average size of AB2 particles using developed algorithm of statistical processing of images from electron microscope. It was found that for all melts mass fraction-time curve has global maximum and the rate of subsequent reduction of mass fraction depends on content of alloying elements.

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Materials Science Forum (Volumes 706-709)

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865-870

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January 2012

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© 2012 Trans Tech Publications Ltd. All Rights Reserved

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