Materials Science Forum Vols. 706-709

Abstract: In the study, novel fabrication processes of functionally-graded (FG) syntactic foams were developed to control distribution of the mechanical properties in the FG foams for highly impact energy absorption. In order to control mechanical properties, the density distributions in FG foams were graded by floating phenomenon of the light-weight micro-balloons in matrix resin during curing process. The density distribution in the foam could be controlled by adjusting the average volume fraction and the turning procedure of the mold before grading the micro-balloons in the foam. The compression tests of the fabricated FG foams suggested that the foams had high absorption of impact energy since the foams collapsed progressively due to the grading of the density distribution.

Abstract: In this research, surface modification of copper with molybdenum was made using explosive welding technique. The underwater shock waves derived from the detonation of explosives was used to bond thin films of molybdenum on copper. Visual observation shows a sound joining of Mo/Cu. Microstructural characterization reveals the bonding interface with a clear wave formation between the participant metals. A clear wavy interface is formed when the weldable conditions lie in the weldability window. When the weldable conditions lie near the right limit or lower limit, a jet trapped region was formed.

Abstract: The various techniques of phase transformation of the material have been proposed by many researchers. We have developed several devices to generate the ultrahigh pressure by using high explosive. One of them uses metal jets. It is expected that the ultrahigh pressure occurs by the head-on collision between metal jets, because the velocity of the metal jet is very high. By mixing a powdered material with metal jets, the pressure of the material becomes high. The purpose of this study is to transform the phase of the powdered material by using this high pressure. The powders of the graphite and hBN were applied. The synthesis to the diamond and cBN was confirmed by X-ray diffraction (XRD). In this paper, the mechanism of the generation of the ultrahigh pressure is explained and the results of the observation of the powder by using scanning transmission electron microscope (STEM) are reported.

Abstract: In this study, the effect of strain rate on the strength and the absorbed energy of polylactic acid resin foam (PLA-foam), which is generally known as one of carbon-neutral and environmentally-friendly polymers, were examined by a series of compression tests at various strain rates from 0.001 to 750 s^-1. For the measurements of the impact load and the displacement of specimen, a special load cell and a high-speed video camera were used, respectively. The flow stress of the PLA-foam strongly depends upon not only strain rate but also density of specimens. Thus, a new technique to eliminate the effect of the difference in the specimen density was proposed and successfully applied. It was also found that the strain-rate dependency of PLA-foam can be expressed by a simple power law.

Abstract: Effect of dislocation behavior on formation of whisker in pure Sn has been investigated. Slip system in β-Sn was determined; slip plane is , and Burgers vector b is . The magnitude of Burgers vector is larger than the smallest interatomic spacing in β-Sn. This means that there is broad space under the extra half plane of edge dislocation. It sould be noted that pipe diffusion along the edge dislocation is enhanced in β-Sn, resulting in easy supply of Sn atoms at the root of Sn whisker [1, 2]. Si-bearing particles, which precipitate on surface of bulk Sn by heat-treatment in quartz tube, suppress the accumulation of both edge and screw dislocations to same area. It is greatly effective for the suppression of the nucleation of Sn whisker.

Abstract: In this study, aluminum alloy A5052 and magnesium alloy AZ31 were joined by conventional parallel setup of explosive welding and underwater explosive welding. Microstructural characterization of conventional welded joints revealed a characteristic wave formation with vortices and contact surface melting layer containing intermetallics. In order to reduce the vortices and melting layer, underwater explosive welding was used. The welding parameters are regulated to reduce the kinetic energy loss during collision. The low kinetic energy loss in underwater explosive welding resulted in the formation of small waves with less vortices and no melting layer.

Abstract: Detonating code, which is a flexible code with an explosive core, is normally used to transmit the ignition of explosives with high detonation velocity 6 km/s. Therefore it is difficult to use detonating code for the explosive welding of common metals toward the detonating direction since the welding velocity exceeds the sound velocity of metals. Hence, an explosive welding method using underwater shock wave generated by the detonation of detonating code was tried. In the present investigation, the details of the experimental setup and results are reported. And the welding conditions are discussed through numerical simulation. From these results it is observed that the above technique is suitable to weld thin metal plates with relatively less explosives.

Abstract: The influence of temperature on crater formation and ejecta composition in thick aluminum alloy targets were investigated for impact velocities ranging from approximately 1.5 to 3.5 km/s using a two-stage light-gas gun. The diameter and depth of the crater increased with increasing temperature. The ejecta size at low temperature was slightly smaller than that at high temperature and room temperature. Temperature did not affect the size ratio of ejecta. The scatter diameter of the ejecta at high temperature was slightly smaller than those at low and room temperatures.

Abstract: An accurate isotropic and kinematic hardening model and description of the strain rate dependent material behaviour is necessary for simulation of fast forming processes. Consequently, the material model parameter identification requires experiments where large strains, high strain rates and strain path changes can be attained. Usually, quasi-static tension-compression Bauschinger tests are used to assess the materials kinematic hardening. Hereby it’s important to have the same specimen geometry and boundary conditions in the forward and reverse loading step which is not easily achieved in high strain rate testing techniques. In this work, high strain rate split Hopkinson bar torsion experiments on Ti6Al4V are carried out to study the constitutive material behaviour at large plastic strain and strain rate. In torsion experiments, due to the absence of cross sectional area reduction, higher strains than in tensile tests can be obtained. In addition, a modified torsional split Hopkinson bar setup is developed to perform dynamic Bauschinger tests. A shear reversed-shear load is applied instead of the classical tension-compression load cycle. The test results are analysed to find out if the technique can be used for characterisation of the kinematic material behaviour. Digital image correlation and finite element simulations are used to improve the interpretation of the experimental results.

Abstract: In this study, a Mg-6wt%Al alloy and its composite containing 0.22vol% Al₂O₃ nanoparticles are fabricated using a disintegrated melt deposition technique, and samples are subjected to quasi-static and dynamic tension. Compared to quasi-static loading, both materials exhibit significantly higher yield stresses and tensile strengths, much better ductility, and thus a higher energy absorption capacity under dynamic tension. In terms of nanoparticle addition, its influence on the mechanical properties are not notable; enhancement of the elastic modulus, yield stress and tensile strength are negligible, and there is a small reduction in ductility. The tensile behaviour obtained in this investigation was compared with results of previous compression tests, and significant tension-compression asymmetry in the response is observed. The tensile yield stress is noticeably larger than that in compression, and the profile of the stress-strain curve for tension differs from that for compression – it is convex upwards for tension, but concave upwards for compression. A possible reason for this asymmetry is the occurrence of twinning in compression and its absence in tension.