Novel High Pressure Multi-Anvil Device for Diamond Production

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Abstract:

The synthesis of diamond crystal from powder mixture of graphite and catalyst alloy is a well known process but it is limited to relatively small crystal dimensions due to the size of the conventional compression chambers. In this work the design and construction of a novel high pressure multi-anvil device with a parallelepiped shaped compression chamber is presented. The design allows the length of the chamber to be limited only by the working space of the press equipment. A four horizontal anvils device was constructed for a specific 2500 ton press with a 600mm working space. The efficiency of this construction was tested in diamond crystal synthesis.

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Materials Science Forum (Volumes 727-728)

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1369-1374

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August 2012

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© 2012 Trans Tech Publications Ltd. All Rights Reserved

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[1] Bundy, F.P., 1962. Basic principles of construction of high pressure apparatus. In: Modern Very High Pressure Techniques. Ed. by Wentorf R.H. Butterworth's, London. Chap. 1, p.9 – 44.

Google Scholar

[2] Tsiklis D., 1976. Techniques of physical-chemical tests under high and ultra high pressure. Ed. Chemistry. Moscow, p.430.

Google Scholar

[3] Spain J.L., 1977. Ultra high pressure apparatus and technology. In: Equipment design, materials and properties. Ed. By J.I. Spain & J. Paauwe. NY. Dekker, pp.395-423 (High pressure technology v. 1).

Google Scholar

[4] Platen B. Von, 1962. Multi-pistons high pressure and high temperature apparatus. In: Modern Very High Pressure Techniques. Ed. by Wentorf R.H. Butterworth's, London. Chap. 6, p.250 – 280, (1962).

Google Scholar

[5] Bundy F.P., 1998b. Ultra high pressure apparatus. Phys. Reports. Vol. 167, No 3, pp.133-176.

Google Scholar

[6] Zeitlin A., 1965a . Equipment for ultra-high pressure. Mechanical Engineering, 87, n 12, p.13.

Google Scholar

[7] Kawai N., 1966. A static high pressure apparatus with tapering multi-pistons forming a sphere. Proc. of Japan Academy. Vol. 42, No 4, pp.385-388.

DOI: 10.2183/pjab1945.42.385

Google Scholar

[8] Witterman W.J., Werkman Th., 1963. Cylindrical high pressure apparatus. Philips Res. Repts. No 18, pp.447-463.

Google Scholar

[9] Bobrovnitchii G.S., Maksimov L. Yu., 1974. Multipiston spherical type device for super high pressure generation. Instruments and Experimental Techniques. Moscow. Vol. 9, 220-222.

Google Scholar

[10] Zeitlin A., 1965b. High pressure technology. Scientific American. 1965. 212, n 5, p.38.

Google Scholar

[11] Tyrner J.M., 1966. High pressure apparatus. Patent No 3239886, C. 18-16.

Google Scholar

[12] Bobrovnitchii G.S., O. K. Nikulin O.K., Belovol V.S., 1992. Device for super high pressure generation. Patent of Russia No 1738322, Cl. B 01j.

Google Scholar

[13] Chepurnov A.I., Fedorov I. I, Sonin V.M. 1997. Experimental modeling of the diamond formation process. Publishing by Siberian RAS SPC UI GGM, Novosibitsk, p.197.

Google Scholar

[14] Bobrovnitchii G.S., Persikov E.S., 2001. The multi-anvil spherical type device of high pressure with cubic compression chamber. In: Sixth applied diamond conference/ Second frontier carbon technology joint conference (ADC/FCT), Auburn, Vol. 1, pp.245-252.

Google Scholar

[15] Bobrovnitchii G.S., 1997. Multi piston installation spherical type for generating high pressures and high temperatures. Patent of Russia No 2077375, Cl. B 01.

Google Scholar