The Influence of Sintering Conditions on Microstructure of La-Ca-Sr-Mn-O Magnetocaloric Ceramics

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Abstract:

A La0.67Ca0.33-xSrxMnO3 (x=0.33; 0.03; 0) perovskite magnetocaloric powders were prepared by solid state synthesis in air. Phase transformations were characterized by thermal analyses and the phase composition was confirmed by X-ray powder diffraction. Pressed pellets were sintered at different temperatures. Microstructure analyses were done by polarized light microscopy and scanning electron microscopy. The influence of sintering conditions on porosity, grain size and content of secondary phases is shown.

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503-506

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April 2014

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© 2014 Trans Tech Publications Ltd. All Rights Reserved

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DOI: 10.1088/0034-4885/68/6/r04

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