Synthesis and Characterization of MCM-41 by XRD, Adsorption Capacity and Foster Swelling Tests

Marcílio Máximo da Silva; Aline Cadigena Lima Patrício; Anna Karoline Freires de Sousa; Meiry Glaúcia Freire Rodrigues; Marta Lígia Pereira da Silva

doi:10.4028/www.scientific.net/MSF.805.657

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HomeMaterials Science ForumMaterials Science Forum Vol. 805Synthesis and Characterization of MCM-41 by XRD,...

Synthesis and Characterization of MCM-41 by XRD, Adsorption Capacity and Foster Swelling Tests

Abstract:

The main objective was to synthesize in the laboratory and characterize the molecular sieve MCM-41. This study has a strong experimental character. The hydrothermal synthesis was performed at 100 ° C for a period of 7 days. The resulting materials were characterized by XRD, EDX, Adsorption Capacity and the Foster Swelling test. Through XRD verified the formation of mesoporous structure. Different organic solvents, namely gasoline, diesel and kerosene were used. The Foster Swelling Test results indicated that the affinity of molecular sieve MCM-41 occurred in the treated clay tested in all organic solvents (gasoline, diesel, kerosene), without and with agitation.

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Materials Science Forum (Volume 805)

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657-661

DOI:

https://doi.org/10.4028/www.scientific.net/MSF.805.657

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Online since:

September 2014

Authors:

Marcílio Máximo da Silva*, Aline Cadigena Lima Patrício, Anna Karoline Freires de Sousa, Meiry Glaúcia Freire Rodrigues, Marta Lígia Pereira da Silva

Keywords:

Adsorption Capacity, Foster’s Swelling, MCM-41, Thermal Treatment, XRD

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References

[1] J. Cui, X. Zhang, H. Liu, S. Liu, K. L. Yeung: J. of Membrane Science, Vol. 325 (2008) p.420.

Google Scholar

[2] R. Shawabkeh, A. Al-Harahsheh, M. Hami, A. Khlaifat: Fuel, Vol. 83, (2004) p.981.

DOI: 10.1016/j.fuel.2003.10.009

Google Scholar

[3] AMCOL, J. W. Darlington, Jr. Marengo, S. E. Yuchs: Process for treating water for removal of oil and water-soluble petroleum oil components. US, Patent number: 5, 922, 206, (1999).

Google Scholar

[4] C. E. Housecroft, E. C. Constable, Chemistry, third ed., Pearson Education Limited, England, (2006).

Google Scholar

[5] O. Kitao, K. E. Gubbins: J. Phy. Chem. Vol. 100 (1996) p.12424.

Google Scholar

[6] J. S. Oh, W. G. Shim, J. W. Lee, J. H. Kim, H. Moon, G. Seo: J. Chem. Eng. Data Vol. 48 (2003) p.1458.

Google Scholar

[7] K. R. O. Pereira, R. A. Hanna, M. M. G. R. Vianna, C. A. R. Pinto, M. G. F. Rodrigues, F. R. Valenzuela- Diaz: Materials Research Vol. 8 (2005) p.77.

Google Scholar

[8] Beck, J.S.; Vartuli, J.C.; Roth, W.J.; Leonowicz, M.E.; Kresge, C.T.; Schmitt, K.D.; Chu, C.T.; Olson, D.H.; Sheppard, E.W.; McCullen, S.B.; Higgins J.B. and Schlenker, J.L., J. Am. Chem. Soc. Vol. 114 (1992) p.10834.

DOI: 10.1021/ja00053a020

Google Scholar

[9] J. C. Vartuli, J. S. Beck: Solid State and Materiails Science Vol. 1 (1996) p.76. x] Montes, A.; Cosenza, E.; Giannetto, G.; Urquieta, E.; Melo, R. A. de; Gnep, N. S. and Guisnet, M., Stud. Surf. Sci. Catal. 117, (1998).

Google Scholar