Hot Solvent Extraction Method for Recycle Epoxy Resin in Waste Printed Circuit Board with Polyethylene Glycol

Article Preview

Abstract:

Waste printed circuit board (WPCB) from waste electrical and electronic equipment (e-waste) can be recycled a precious metal part while a non-metal part was burned or landfilled, which normally generated toxic substance of organic component to environment. The research work aimed to recycle epoxy resin by hot solvent chemical extraction. Polyethylene glycol 400 (PEG400) and ethylene glycol (EG), at 180°C, were mainly using as solvent and sodium hydroxide (NaOH) as a catalyst. Extraction method was reflux technique. The thermogravimetric analysis (TGA), Specific viscosity, and Fourier transform infrared spectroscopy (FT-IR) methods were investigated and discussed. The TGA result showed that the organic composition was 40.73%wt. The maximum of percent yield was 97.89% at non-metal WPCB/PEG, equal to 0.05 g/ml. Moreover, the extracted product presented a functional group close to virgin epoxy resin according to the peak of FT-IR data. The recycled epoxy resin could be formed well on specimen by virgin epoxy resin and hardener filled with 50% recycled extraction product.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

524-529

Citation:

Online since:

May 2016

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2016 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

* - Corresponding Author

[1] C. Jirang, Z. Lifeng, Metallurgical recovery of metals from electronic waste: A review, J. Hazard. Mater. 158 (2008) 228-256.

Google Scholar

[2] K. Huang, J. Guo, Z. Xu, Recycling of waste printed circuit boards: A review of current technologies and treatment status in China, J. Hazard. Mater. 164 (2009) 399-408.

DOI: 10.1016/j.jhazmat.2008.08.051

Google Scholar

[3] J. Wu, J. Li, Z-M. Xu, A new two-roll electrostatic separator for recycling of metals and nonmetals from waste priented circuit board, J. Hazard. Mater. 161 (2009) 257-262.

DOI: 10.1016/j.jhazmat.2008.03.088

Google Scholar

[4] Y. Zhou, K. Qiu, A new technology for recycling material from waste printed circuit boards, J. Hazard. Mater. 175 (2010) 823-828.

DOI: 10.1016/j.jhazmat.2009.10.083

Google Scholar

[5] Coombs, C. F. and Jr, Printed circuits handbook, sixth ed., McGraw-Hill, United States of America, (2008).

Google Scholar

[6] J. Li, H. Lu, J. Guo, Z. Xu, Y. Zhou, Recycling technology for recovering resources and products from waste printed circuit boards, Environ. Sci. Technol. 41 (2007) 1995-(2000).

DOI: 10.1021/es0618245

Google Scholar

[7] R. Dangtungee, S. Somchua, S. Siengchin, Recycling glass fiber/epoxy resin of waste printed circuit boards: morphology and mechanical properties, Mech. Compos. Mater. 48 (2012) 325-330.

DOI: 10.1007/s11029-012-9279-1

Google Scholar

[8] P. Zhu, Y. Chen, L.Y. Wang, M. Zhou, J. Zhou, The separetion of waste printed circuit board by dissolving bromine epoxy resin using organic solvent, Waste. Manag. 33 (2013) 484-488.

DOI: 10.1016/j.wasman.2012.10.003

Google Scholar

[9] R. Dangtungee, S. Siengchin, C. Kitpaosong, Novel method for recycle epoxy resin from waste printed circuit board, Adv. Mat. Res. 931-932 (2014) 90-94.

DOI: 10.4028/www.scientific.net/amr.931-932.90

Google Scholar

[10] P. Yang, Q. Zhou, X.X. Yuan, J.M.N. van Kasteren, Y.Z. Wang, Highly efficient solvolysis of epoxy resin using poly(ethylene glycol)/NaOH system, Polym. Degrad. Stab. 97 (2012) 1101-1106.

DOI: 10.1016/j.polymdegradstab.2012.04.007

Google Scholar

[11] C. Kitpaosong, S. Seeyangnok, R. Dangtungee, Recycling epoxy resin from waste printed circuit board via chemical process, in: PACCON2014 proceeding, Chemical Society of Thailand, Khon Kean, Thailand, 2014, pp.988-991.

DOI: 10.4028/www.scientific.net/amr.931-932.90

Google Scholar