Fracture Properties of Mg-Alloys Assessed with Nanoindentation

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This paper deals with micromechanical properties of biocompatible magnesium alloys MgCa0.8 prepared by extrusion. At first, the microstructure, elastic and hardness properties are assessed at the scale of one micrometer by means of a nanoindenter. Further, determination of fracture mechanism, fracture area and fracture toughness of the alloy is studied with sharp indentation, optical microscopy and SEM and by means of energetic methods. Based on the examination of optical images it was concluded that the Mg matrix is not vulnerable to distinct cracking around indents even for high indentation loads. By computations, it was found the fracture area is very small, about 0.7-3% of the tip contact area based on the assumption of limit values of the target fracture toughness 10-20 MPa·m1/2.

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257-262

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March 2017

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© 2017 Trans Tech Publications Ltd. All Rights Reserved

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[1] J. Němeček, V. Králík, J. Vondřejc, Micromechanical analysis of heterogeneous structural materials, Cem Concr Comp 36 (2013) 85-92.

DOI: 10.1016/j.cemconcomp.2012.06.015

Google Scholar

[2] W.R.L. Da Silva, J. Němeček, P. Štemberk, Methodology for nanoindentation-assisted prediction of macroscale elastic properties of high performance cementitious composites, Cem Concr Comp 45 (2014) 57-68.

DOI: 10.1016/j.cemconcomp.2013.09.013

Google Scholar

[3] J. Minster, O. Bláhová, J. Lukeš, et al., Time-dependent mechanical characteristics measured through the use of a microindentation technique, Mech Time-Dep Mat 14 (3) (2010) 243-251.

DOI: 10.1007/s11043-009-9105-x

Google Scholar

[4] M. Sebastiani, K.E. Johanns, E.G. Herbert, G.M. Pharr, Measurement of fracture toughness by nanoindentation methods: Recent advances and future challenges, Current Opinion in Solid State and Materials Science 19 (2015) 324–333.

DOI: 10.1016/j.cossms.2015.04.003

Google Scholar

[5] B.R. Lawn, A.G. Evans, D.B. Marshall, Elastic/plastic indentation damage in ceramics: the median/radial crack system, J. Am. Ceram. Soc. 63 (1980) 574–581.

DOI: 10.1111/j.1151-2916.1980.tb10768.x

Google Scholar

[6] J. Chen, S.J. Bull, Indentation fracture and toughness assessment for thin optical coatings on glass. J. Phys. D-Appl. Phys. 40 (2007) 5401–5417.

DOI: 10.1088/0022-3727/40/18/s01

Google Scholar

[7] J.S. Field, M.V. Swain, R.D. Dukino, Determination of fracture toughness from the extra penetration produced by indentation-induced pop-in, J. Mater. Res. 18 (2003) 1412.

DOI: 10.1557/jmr.2003.0194

Google Scholar

[8] Y.T. Cheng, Z.Y. Li, C.M. Cheng, Scaling relationships for indentation measurements, Philos. Mag. A 82 (2002) 1821–1829.

Google Scholar

[9] A. Milenin, M. Gzyl, T. Rec, B. Plonka, Computer aided design of wires extrusion from biocompatible Mg-Ca magnesium alloy, Archives of Metal. and Mater. 59(2) (2014) 551–556.

DOI: 10.2478/amm-2014-0091

Google Scholar

[10] W. Oliver, G. Pharr, An Improved Technique for Determining Hardness and Elastic-Modulus using Load and Displacement Sensing Indentation Experiments, J. Mater. Res. 7 (1992) 1564-1583.

DOI: 10.1557/jmr.1992.1564

Google Scholar

[11] J. Bočan, J. Maňák, A. Jäger, Nanomechanical analysis of AZ31 magnesium alloy and pure magnesium correlated with crystallographic orientation, Materials Science and Engineering A 644 (2015) 121–128.

DOI: 10.1016/j.msea.2015.07.055

Google Scholar

[12] H. Somekawa, T. Mukai, Effect of grain refinement on fracture toughness in extruded pure magnesium, Scripta Materialia 53 (2005) 1059–1064.

DOI: 10.1016/j.scriptamat.2005.07.001

Google Scholar