Effect of Thermomechanical Processing on Grain Size, Texture and Mechanical Properties of Pure Magnesium

Article Preview

Abstract:

This study aims to investigate the effect of processing routes (A and Bc) and temperature on microstructure, texture and mechanical properties of pure magnesium was studied in this research. An extruded pure magnesium (~99,9 %) was subjected to severe plastic deformation (SPD) by ECAP. Deformation was conducted at 523K and 473K and two different processing routes (A and Bc) were used to control the texture. The microstructure and texture characterization of the pressed materials were carried out. It was found that the microstructure displayed a bimodal grain structure after two passes and then became homogeneous after four passes following both routes A and Bc. The misorientation distribution was examined and the results revealed that the fraction of high angle grain boundaries (HAGB) was higher at temperature 473K. The texture was randomized following route Bc whereas it became strengthened in route A after four passes. According to the Hall-Petch (HP) relationship, the yield stress of polycrystalline metals increases with a decrease in grain size. In this study, a positive slope k was achieved in the strengthened texture while a negative one was obtained in the softened texture. The ductility of ECAP processed material was considerably improved (from 23% to 38%) without sacrificing the yield stress by route Bc at 423K.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

97-108

Citation:

Online since:

April 2020

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2020 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

* - Corresponding Author

[1] Ding, S. X., Lee, W. T., Chang, C. P., Chang, L. W. and Kao, P. W., Improvement of strength of magnesium alloy processed by equal channel angular extrusion, Scripta Materialia, Vol.59, No.9, (2008), pp.1006-1009.

DOI: 10.1016/j.scriptamat.2008.07.007

Google Scholar

[2] Fan, G., Zheng, M. Y., Hu, X. S., Xu, C., Wu, K., and Golovin, I. S., Improved mechanical property and internal friction of pure Mg processed by ECAP. Materials Science & Engineering A, Vol.556, (2012), pp.588-594.

DOI: 10.1016/j.msea.2012.07.031

Google Scholar

[3] Tong, L.B., Zheng, M. Y., Hua, X.S., Wu, K., Xu, S. W., Kamado, S. and Kojima, Y., Influence of ECAP routes on microstructure and mechanical properties of Mg–Zn–Ca alloy. Materials Science & Engineering A, Vol.527 (2010) p.4250–4256.

DOI: 10.1016/j.msea.2010.03.062

Google Scholar

[4] Furukawa, M., Iwahashi, Y., Horita, Z., Nemoto, M. and Langdon, T. G., The shearing characteristics associated with equal-channel angular pressing, Materials Science and Engineering A257, (1998), pp.328-332.

DOI: 10.1016/s0921-5093(98)00750-3

Google Scholar

[5] Gan, W. M., Zhenga, M. Y., Chang, H., Wang, X. J., Qiao, X. G., Wu, K. B. Schwebke and Brokmeier, H. G., Microstructure and tensile property of the ECAPed pure magnesium, Journal of Alloys and Compounds, Vol.470, No.1-2, (2009), pp.256-262.

DOI: 10.1016/j.jallcom.2008.02.030

Google Scholar

[6] Iwahashi, Y., Wang, J., Horita, Z., Nemoto, M. and Langdon, T. G. Principle of equal-channel angular pressing for the processing of ultra-fine grained materials, Scripta Materialia, Vol.35, No.2, (1996), pp.143-146.

DOI: 10.1016/1359-6462(96)00107-8

Google Scholar

[7] Krajnak, T., Minarik, P., Straska, J., Gubicza, J. Mathis, K., and Janecek, M., Influence of equal channel angular pressing temperature on texture, microstructure and mechanical properties of extruded AX41 magnesium, Journal of Alloys and Compounds, Vol.705, (2017), pp.273-282.

DOI: 10.1016/j.jallcom.2017.02.061

Google Scholar

[8] Li, Z., Zhou, S., and Huang, N., Effect of ECAE processing temperature on the microstructure, mechanical properties and corrosion behavior of pure magnesium. International Journal of Minerals, Metallurgy, and Materials, Vol.22, No.6, (2015), pp.639-647.

DOI: 10.1007/s12613-015-1117-8

Google Scholar

[9] Nakashima, K., Horita, Z., Nemoto, M. and Langdon, T.G., Development of a multi-pass facility for equal-channel angular pressing to high total strains, Materials Science and Engineering: A Vol.281, No.1–2, (2000), pp.82-87.

DOI: 10.1016/s0921-5093(99)00744-3

Google Scholar

[10] Rao, G. S. and Prasad, Y. V. R. K., Grain Boundary Strengthening in Strongly Textured Magnesium Produced by Hot Rolling, Metallurgical Transactions A, Vol.13, No.12 (1982), pp.2219-2226.

DOI: 10.1007/bf02648393

Google Scholar

[11] Valiev, R. Z., and Langdon, T. G., Principles of equal-channel angular pressing as a processing tool for grain refinement, Progress in Materials Science, Vol.51, No.7, (2006), pp.881-981.

DOI: 10.1016/j.pmatsci.2006.02.003

Google Scholar

[12] Wang, Y. N. and Huang, J. C., Grain Size Dependence of Yield Strength in Randomly Textured Mg-Al-Zn Alloy, Materials Transactions, Vol.48, No.2, (2007) pp.184-188.

DOI: 10.2320/matertrans.48.184

Google Scholar

[13] Satyam, S., Gottstein, G. and Kumar, R., Evolution of crystallographic texture during equal channel angular extrusion (ECAE) and its effects on secondary processing of magnesium, Materials Science and Engineering A, Vol.471 (2007), pp.1-14.

DOI: 10.1016/j.msea.2007.05.030

Google Scholar

[14] Poggiali, F. S. J., Figueiredo, R. B., Aguilar, M. T. P., and Cetlin, P. R., Grain refinement of commercial purity magnesium processed by ECAP. Materials Research, Vol.15, No.2, (2012), pp.312-316.

DOI: 10.1590/s1516-14392012005000022

Google Scholar

[15] Ho-Kyung Kim, The grain size dependence of flow stress in an ECAPed AZ31 Mg alloy with a constant texture. Materials Science and Engineering A, Vol.515, (2009), pp.66-70.

DOI: 10.1016/j.msea.2009.02.039

Google Scholar

[16] Ono, N., Nowak, R. and Miura, S., Effect of deformation temperature on Hall-Petch relationship registered for polycrystalline magnesium. Materials Letters, Vol.58, (2003), pp.39-43.

DOI: 10.1016/s0167-577x(03)00410-5

Google Scholar

[17] Venkatachalam P., Ramesh Kumar S., Ravisankar B., Thomas Paul V., Vijayalakshmi M., Effect of processing routes on microstructure and mechanical properties of 2014 Al alloy processed by equal channel angular pressing. Transactions of Nonferrous Metals Society of China 20 (2010), pp.1822-1828.

DOI: 10.1016/s1003-6326(09)60380-0

Google Scholar

[18] Joung Sik Suh (2015), Improvement in Cold Formability of AZ31 Magnesium Alloy Sheets Processed by Equal Channel Angular Pressing (ECAP). Technical University of Munich, Dissertation. p.4.

DOI: 10.1016/j.jmatprotec.2014.11.029

Google Scholar

[19] Hall, E.O., The Deformation and Ageing of Mild Steel: III Discussion of Results Proceedings of the Physical Society, Vol. 64, (1951) p.747–753.

DOI: 10.1088/0370-1301/64/9/303

Google Scholar