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Microwave-Assisted Combustion Synthesis of α-Alumina and Magnesium Aluminate Spinel Nanocomposite Powders
Abstract:
Microwave-assisted combustion synthesis of α-alumina-magnesium spinel nanocomposite powders from a route using ammonium aluminum carbonate hydroxide (AACH) as a precursor was studied. γ- to α-phase transformation temperature of microwave-assisted alumina composite powders is lowered by 100°C compared to that of normal heat-treated alumina composite powders. The crystallite size of the microwave-assisted composite powders was considerably decreased from 42 nm to 29 nm compared to that of the normal heat treated composite powders. Nanosized α- alumina-magnesium aluminate composite powders were successfully synthesized by microwave-assisted combustion under nitrogen atmosphere at 1050°C.
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191-194
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January 2007
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© 2007 Trans Tech Publications Ltd. All Rights Reserved
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