Synthesis and Characterization of Magnesium Diboride Additions of Bi-2223 on the Microstructure and Superconducting Transition

Arlina Ali; Abdul Halim Shaari; Soo Kien Chen; Julie Juliewatty Mohamed; Nurul’ain Mohd Kamal; Mohd Mustafa Awang Kechik

doi:10.4028/www.scientific.net/SSP.290.233

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Synthesis and Characterization of Magnesium Diboride Additions of Bi-2223 on the Microstructure and Superconducting Transition

Abstract:

In this paper, solid state method was using to synthesize the of magnesium diboride (MgB₂) added in Bi _1.6Pb _0.4Sr₂Ca₂Cu₃O_δ(Bi-2223) superconductor from 0.00 to 0.10 wt.%. The effect on additions were investigated through X-ray Diffraction (XRD), resistance-temperature (R-T) measurement and Scanning Electron Microscope (SEM). From the XRD result, volume fraction of Bi-2223 showed the highest volume percentage was 76 % correspond to addition with MgB₂=0.02 wt.% and slightly decreased the percentage while increased the additions. From the R-T measurement, all samples showed the metallic behavior in the normal state. Morphology images showed that the grains were flaky plates and the size slightly increased. These results revealed that, additions of magnesium diboride change the microstructure and decrease the superconducting transition.

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Periodical:

Solid State Phenomena (Volume 290)

Pages:

233-238

DOI:

https://doi.org/10.4028/www.scientific.net/SSP.290.233

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Online since:

April 2019

Authors:

Arlina Ali*, Abdul Halim Shaari, Soo Kien Chen, Julie Juliewatty Mohamed, Nurul’ain Mohd Kamal, Mohd Mustafa Awang Kechik

Keywords:

Bi-2223, Magnesium Diboride, Magnesium Synthesis, Superconducting Transition

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