Oxidation Kinetic and Oxide Scale Morphology of Fe-33Ni-19Cr Ni-Based Superalloy

Abstract:

In the present study, outcome of various grain size of heat treated Fe-33Ni-19Cr Ni-based superalloy at high temperature cyclic oxidation condition was investigated. The Fe-33Ni-19Cr Ni-based superalloy was experienced a series of heat treatment process at two assorted temperatures, which are 1000 °C and 1100 °C, soaking for 3 hours and then rapid cooled by water quench. The heat treatment process produced a fine and coarse grain size structure. The cyclic oxidation test was performed for both heat treated samples at 700 °C under cyclic conditions in the laboratory air for 150 cycles. The weight change was measured discontinuously at different cycles to identify the kinetics of oxidation. SEM and FESEM outfitted with EDX spectrometer were utilized to analyzed the oxidation product. As a result, the weight change increased with time, with fine grain HT1000 sample recorded lower weight gain compared to coarse grain HT1100 sample. In addition, both sample formed uniform and continuous oxide scale on the alloy surface.

• Periodical: Solid State Phenomena (Volume 336)
• Pages: 3-9
• DOI: https://doi.org/10.4028/p-j0a5a5
• Online since: August 2022
• Authors: Noraziana Parimin*, Esah Hamzah
• Keywords: Alloy 800H, Cyclic Oxidation, Heat Treatment, Ni-Based Superalloy, Oxidation Kinetic

References

[1] J. Jiang, G. Xiao, Y. Wang, Y. Liu, High temperature oxidation behavior of the wrought Ni-based superalloy GH4037 in the solid and semi-solid state, J. of Alloys & Comp. 784 (2019) 394-404.

DOI: 10.1016/j.jallcom.2019.01.093

[2] C.N. Athreya, K. Deepak, Dong-Ik Kim, B. de Boer, S. Mandal, V.S. Sarma, Role of grain boundary engineered microstructure on high temperature steam oxidation behaviour of Ni based superalloy alloy 617, J. of Alloys & Comp. 778 (2019) 224-233.

DOI: 10.1016/j.jallcom.2018.11.137

[3] J. Cao, J. Zhang, R. Chen, Y. Ye, Y. Hua, High temperature oxidation behavior of Ni-based superalloy GH202, Mater. Charac. 118 (2016) 122-128.

DOI: 10.1016/j.matchar.2016.05.013

[4] L.J. Chen, P.K. Liaw, H. Wang, Y.H. He, R.L. McDaniels, L. Jiang, B. Yang, D.L. Klarstrom, Cyclic deformation behavior of HAYNES® HR-120® superalloy under low-cycle fatigue loading, Mech. of Mater. 36 (1-2) (2004) 85-98.

DOI: 10.1016/s0167-6636(03)00033-4

[5] B.R. Barnard, P.K. Liaw, R.A. Buchanan, D.L. Klarstrom, Affects of applied stresses on the isothermal and cyclic high-temperature oxidation behavior of superalloys, Mater. Sci. & Eng.: A. 527 (16-17) (2010) 3813-3821.

DOI: 10.1016/j.msea.2010.03.050

[6] N. Parimin, E. Hamzah, Oxidation kinetics of Fe-Ni-Cr Alloy at 900 °C, Mater. Sci. Forum 1010 (2020) 58-64.

DOI: 10.4028/www.scientific.net/msf.1010.58

[7] N. Parimin, E. Hamzah, Effect of solution treatment temperature on the microstructure of Fe-33Ni-19Cr alloy, Mater. Sci. Forum 1010 (2020) 21-27.

DOI: 10.4028/www.scientific.net/msf.1010.21

[8] N. Parimin, E. Hamzah, Influence of Solution Treatment Temperature on the Microstructure of Ni-based HR-120 Superalloy, IOP Conf. Ser.: Mater. Sci. Eng. 957 (2020) 012003.

DOI: 10.1088/1757-899x/957/1/012003

[9] L. Tan, Corrosion behavior of Ni-base alloys foe advanced high temperature water-cooled nuclear plants, Cor. Sci. 50 (11) (2008) 3056-3062.

DOI: 10.1016/j.corsci.2008.08.024

[10] A.M. de Sousa Malafaia, M.F. de Oliveira, Anomalous cyclic oxidation behaviour of a Fe-Mn-Si-Cr-Ni shape memory alloy, Cor. Sci. 119 (2017) 112-117.

DOI: 10.1016/j.corsci.2017.02.026

[11] D. Saber, I.S. Emam, R. Abdel-Karim, High temperature cyclic oxidation of Ni based superalloys at different temperatures in air, J. of Alloys & Comp. 719 (2017) 133-141.

DOI: 10.1016/j.jallcom.2017.05.130

[12] N. Parimin, E. Hamzah, High temperature cyclic oxidation of Ni-based 800H superalloy at 700°C, IOP Conf. Ser.: Mater. Sci. Eng. 957 (2020) 012013.

DOI: 10.1088/1757-899x/957/1/012013

[13] N. Birks, G.H. Meier, F.S. Petit, Introduction to the high-temperature oxidation of metals, second ed., Cambridge University Press, United Kingdom, (2006).

[14] J. Zurek, D.J. Young, E. Essuman, M. Hansel, H.J. Penkalla, L. Niewolak, W.J. Quadakkers, Growth and adherence of chromia based surface scales in NI-base alloys in HIgh- and Low-pO2 gases, Mater. Sci. Eng. A 477 (2008) 259-270.

DOI: 10.1016/j.msea.2007.05.035

[15] D.J. Young, J. Zurek, L. Singheiser, W.J. Quadakkers, Temperature dependence of oxide scale formation on high-Cr ferritic steels in Ar-H2-H2O, Corros. Sci. 53 (2011) 2131-2134.

DOI: 10.1016/j.corsci.2011.02.031

[16] L. Tan, X. Ren, K. Sridharan, T.R. Allen, Effect of shot-peening on the oxidation of Alloy 800H exposed to supercritical water and cyclic oxidation, Corros. Sci. 50 (2008) 2040-2046.

DOI: 10.1016/j.corsci.2008.04.008