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Online since: May 2022
Authors: Carmine Sileno, Diego Calvo Ruiz
It features bonding structures, which are abrasive grains bond in a vitrified matrix system.
With this approach, the same number of grains are active in the work zone.
When material removal takes place on the substrate, new, sharp diamond grains are introduced by the matrix system.
With this approach, the same number of grains are active in the work zone.
When material removal takes place on the substrate, new, sharp diamond grains are introduced by the matrix system.
Online since: January 2013
Authors: Lan Li Chen, Sheng Zhao Wang, Ming Ji Shi, Hai Hong Wang, Wen Fang Si
But because of the small number of holes, the porosity is small, so the silicon wall between adjacent pores is thicker.
Because in this process, the growth of porous silicon was accelerated and larger silicon grains were formed.
Then smaller grains were formed and he peaks of PL blue shifted.
As a result, larger silicon grains were formed and the peaks of PL will red shift.
Because in this process, the growth of porous silicon was accelerated and larger silicon grains were formed.
Then smaller grains were formed and he peaks of PL blue shifted.
As a result, larger silicon grains were formed and the peaks of PL will red shift.
Online since: December 2012
Authors: Xiao Chun Ma, Lei Hao Cui, Guang Fei Xu
Table 2 The influence of reunite by addition of PEG
number
addition
phenomenon of reunion and stratified
1
0
some black mass, stratified
2
1
little black mass
3
2
turbid liquid
4
4
turbid liquid
a (PEG 0g) b (PEG 2g)
Fig. 2 The TEM image of different addition of PEG
The TEM images are similar to the phenomenon described above.
From image (a), the Fe3O4 particles reunite seriously without PEG; from image (b), the Fe3O4 particles disperse well and the grain size is 10nm-20nm.
According to the D=kλ/βcosθ, the average grain size can be work out.
In this paper, the average grain size is about 10nm-50nm.
From image (a), the Fe3O4 particles reunite seriously without PEG; from image (b), the Fe3O4 particles disperse well and the grain size is 10nm-20nm.
According to the D=kλ/βcosθ, the average grain size can be work out.
In this paper, the average grain size is about 10nm-50nm.
Online since: June 2014
Authors: Lei Zhang, Xi Bao Chen, Hong Bo Shan, Xue Lei Wu, Yan Min Zhao
Figure 2 Split fracture source and propagation direction (arrow direction)
1.2 Turboshaft Fracture Morphology Analysis by Scanning Electron Microscopy By scanning electron microscopy, the fracture source area was fine dimples (about 0.8mm range from the outer surface) + mixed topography along the grain, dimple (from the outer surface of the range of approximately 0.8 to 1.5mm), fracture morphology as shown in Fig.3.
Fine dimples Along the grain + dimples Fig.3 Fracture morphology of the source region From the failure of the turboshaft fracture analysis, fracture originated in the outer surface of the root of the turboshaft splines, no obvious source of mechanical damage, microscopic primarily in a small number of dimples along the grain + mixed morphology, so the turboshaft is a brittle fracture.
Fine dimples Along the grain + dimples Fig.3 Fracture morphology of the source region From the failure of the turboshaft fracture analysis, fracture originated in the outer surface of the root of the turboshaft splines, no obvious source of mechanical damage, microscopic primarily in a small number of dimples along the grain + mixed morphology, so the turboshaft is a brittle fracture.
Online since: November 2007
Authors: Thomas Oberbach, Sabine Begand, Wilfried Glien
Number Wt % Al2O3 Wt % ZrO2
DC 0 100 0
DC 20 80 20
DC 25 75 25
DC 30 70 30
DC 40 60 40
DC 60 40 60
DC 80 20 80
DC 100 0 100
Table 1: Overview of utilised mixtures
Especially the mixture DC 25 and DC 80 compared to the other mixtures and the pure oxides in the
binary system Al2O3-ZrO2 are a matter of particular interest regarding their potential for
endoprothetic applications. [1,2]
Test specimens were formed by means of slip casting.
The density determination according to the Archimedes principle resulted (for all mixtures) in a relative sintering density of > 99.5 %, with grain sizes of 300 - 800 nm for the dispersion ceramics.
DC 0 DC 25 DC 60 DC 100 Figure 1: Microstructure of selected ceramics The grain size (table 2) of alumina can be reduced by dispersion with ZrO2 from 1.57 µm to 0.34 µm in the mixture 20 % Al2O3 - 80% ZrO2 (DC 80).
DC 0 DC 20 DC 25 DC 30 DC 40 DC 60 DC 80 DC100 Al2O3 1.57 µm 0.73 µm 0.60 µm 0.57 µm 0.57 µm 0.50 µm 0.34 µm − Y-TZP − 0.35 µm 0.31 µm 0.45 µm 0.41 µm 0.52 µm 0.41 µm 0.40 µm Table 2: Median Grain size of all used ceramics The elastic characteristics such as thermal conductivity and Young´s modulus comply with the relations of the structure-property correlations (1 st order limit curves), i.e. with increasing ZrO2 portion, these parameters are characterized by a linear decrease.
The density determination according to the Archimedes principle resulted (for all mixtures) in a relative sintering density of > 99.5 %, with grain sizes of 300 - 800 nm for the dispersion ceramics.
DC 0 DC 25 DC 60 DC 100 Figure 1: Microstructure of selected ceramics The grain size (table 2) of alumina can be reduced by dispersion with ZrO2 from 1.57 µm to 0.34 µm in the mixture 20 % Al2O3 - 80% ZrO2 (DC 80).
DC 0 DC 20 DC 25 DC 30 DC 40 DC 60 DC 80 DC100 Al2O3 1.57 µm 0.73 µm 0.60 µm 0.57 µm 0.57 µm 0.50 µm 0.34 µm − Y-TZP − 0.35 µm 0.31 µm 0.45 µm 0.41 µm 0.52 µm 0.41 µm 0.40 µm Table 2: Median Grain size of all used ceramics The elastic characteristics such as thermal conductivity and Young´s modulus comply with the relations of the structure-property correlations (1 st order limit curves), i.e. with increasing ZrO2 portion, these parameters are characterized by a linear decrease.
Online since: August 2022
Authors: Gehad Genidy Mohamed, Sameh Hamed Ismail, Ahmed Roshdy Elsakhry, Mohamed Kamal Khalaf, Mostafa Abdel-Hamied
The characterization process for the prepared core-shell showed the smoothness and spherical shape of the grains with approximate size of 72 nm.
It should be noted that ethyl silicate-based consolidation products have a number of drawbacks, including chemical incompatibility with treated limestone, where the surfaces of carbonate grains lack the ability to react with the consolidant used, and the action of silica gel formed after polymerization is assumed to be merely that of a compacting agent, acting as a filler of stone voids, and a lack of chemical bonding between the consolidant and the treated limestone [10].
In contrast, the use of nanolime (Ca(OH)2) in limestone consolidation provides a number of advantages, including total chemical compatibility with the calcitic substrate, which allows stone grains to link together to reinforce the stone [10].
Porosity expresses the relationship between the size of the spaces between the grains of the material.
The smoothness and spherical shape of the lime-silica core-shell nanostructures grains were also disclosed using these methods.
It should be noted that ethyl silicate-based consolidation products have a number of drawbacks, including chemical incompatibility with treated limestone, where the surfaces of carbonate grains lack the ability to react with the consolidant used, and the action of silica gel formed after polymerization is assumed to be merely that of a compacting agent, acting as a filler of stone voids, and a lack of chemical bonding between the consolidant and the treated limestone [10].
In contrast, the use of nanolime (Ca(OH)2) in limestone consolidation provides a number of advantages, including total chemical compatibility with the calcitic substrate, which allows stone grains to link together to reinforce the stone [10].
Porosity expresses the relationship between the size of the spaces between the grains of the material.
The smoothness and spherical shape of the lime-silica core-shell nanostructures grains were also disclosed using these methods.
Online since: November 2020
Authors: Naresh Kumar Konada, B.B.Ashok Kumar, Roopsandeep Bammidi, K.N.S. Suman
Scanning electron microscope images (SEM) are observed for the samples to observe the grain distribution present in the composite.
The impact strength of (0.28J/mm2) and Vickers hardness number of 43.89 is also better compared to other samples.
The grain distributions of AF1 and AF2 samples indicated in fig 16(b) and fig 16 (c) was also poor.
The grains are not distributed uniformly across the composite.
Comparing the SEM results of all the samples AF4 sample specimen grains are uniformly distributed and randomly arranged and the grains are also not disturbed too much under the action of forces acting on the sample specimen.
The impact strength of (0.28J/mm2) and Vickers hardness number of 43.89 is also better compared to other samples.
The grain distributions of AF1 and AF2 samples indicated in fig 16(b) and fig 16 (c) was also poor.
The grains are not distributed uniformly across the composite.
Comparing the SEM results of all the samples AF4 sample specimen grains are uniformly distributed and randomly arranged and the grains are also not disturbed too much under the action of forces acting on the sample specimen.
Online since: August 2012
Authors: Pei Sun, Zhigang Zak Fang
Thermomechanical processes, i.e. hot/cold working plus heat treatments may also be used to refine grain size and achieve desired phase composition and morphology.
In short, although PM Ti has great potentials as low-cost alternative for Ti manufacturing, a number of issues still plague PM Ti and prevent its acceptance in the industry.
Using the new process, Ti powders can be sintered to greater than 99% dense with as-sintered grain size being approximately one micrometer or less for Ti-6Al-4V.
Based on SEM and TEM images, the mean grain size of β phases is about 0.5 μm and the mean grain size of α phase is about 1 μm.
Wang, Hydrogen Sintering of Titanium to Produce High Density Fine Grain Titanium Alloys, Adv.
In short, although PM Ti has great potentials as low-cost alternative for Ti manufacturing, a number of issues still plague PM Ti and prevent its acceptance in the industry.
Using the new process, Ti powders can be sintered to greater than 99% dense with as-sintered grain size being approximately one micrometer or less for Ti-6Al-4V.
Based on SEM and TEM images, the mean grain size of β phases is about 0.5 μm and the mean grain size of α phase is about 1 μm.
Wang, Hydrogen Sintering of Titanium to Produce High Density Fine Grain Titanium Alloys, Adv.
Online since: June 2014
Authors: Bin Fang, Xiao Qing Li, Ming Xu
In recent decades,domestic and international materials academics carried out a large number of researches on the high brittleness of Al2O3 ceramics.
(ACT1) (ACT2) (ACT3) (ACT4) (ACT5) (ACT6) Fig.3.SEM microstructure of fracture SEM microstructure of little reunion is figure 4.We can see that matrix grain combine closely, distribution of grain size is uniform,the main form of fracture is intergranular fracture.When volume fraction of carbon nanotubes is little low , carbon nanotubes pin in the alumina substrate, make the density of material better;with increasing the content of carbon nanotubes ,carbon nanotubes in composites matrix will lead to big groups, and appear some disorderly lamellar sediments of graphite in the junctions of grain, make the stability of interface poor, the performance of the material is affected.
(ACT1) (ACT2) (ACT3) (ACT4) (ACT5) (ACT6) Fig.3.SEM microstructure of fracture SEM microstructure of little reunion is figure 4.We can see that matrix grain combine closely, distribution of grain size is uniform,the main form of fracture is intergranular fracture.When volume fraction of carbon nanotubes is little low , carbon nanotubes pin in the alumina substrate, make the density of material better;with increasing the content of carbon nanotubes ,carbon nanotubes in composites matrix will lead to big groups, and appear some disorderly lamellar sediments of graphite in the junctions of grain, make the stability of interface poor, the performance of the material is affected.
Online since: February 2007
Authors: Qing Rui Yin, Xi Yun He, Yong Zhang, Zi Ping Cao, Ai Li Ding
The SEM micrographs of fracture surfaces indicated a
high dense material consisting of uniform equiaxed grains
(Fig.3).
The grain size decreases slightly as x increased.
This can be explained by noting that, when the doping amount increased, some of Dy 3+ entered into the B site of ABO3 structure to produce oxygen vacancies, which would restrict the grain growth.
Vol.25. (1990), pp539. 0 200 400 600 800 1000 1200 [Pb0.88 (La1-xDyx)0.12] (Zr0.40 Ti0.60)O3 x=0 x=0.1 x=0.2 x=0.4 x=0.3 INTENSITY(a.u) WAVE NUMBER (cm -1 ) Fig.4 Raman spectra of PLDZT ceramics
The grain size decreases slightly as x increased.
This can be explained by noting that, when the doping amount increased, some of Dy 3+ entered into the B site of ABO3 structure to produce oxygen vacancies, which would restrict the grain growth.
Vol.25. (1990), pp539. 0 200 400 600 800 1000 1200 [Pb0.88 (La1-xDyx)0.12] (Zr0.40 Ti0.60)O3 x=0 x=0.1 x=0.2 x=0.4 x=0.3 INTENSITY(a.u) WAVE NUMBER (cm -1 ) Fig.4 Raman spectra of PLDZT ceramics