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Online since: September 2021
Authors: Lusiana Lusiana, Cokorda Istri Putri Kusuma Kencanawati, Tjokorda Gde Tirta Nindhia, Dewa Ngakan Ketut Putra Negara, I Made Widiyarta, I Made Astika
The final stage is the activation process proposing to increase the pore structure of charcoal [28].
Journal of Physics and Chemistry of Solids, 74(6), 886-891. https://doi.org/10.1016/j.jpcs.2013.01.036 [22] Das, D., Samal, D.
Preparation, Surface and Pore Structure of High Surface Area Activated Carbon Fibers from Bamboo by Steam Activation.
Modification of the porous structure along the preparation of activated carbon monoliths with H3PO4 and ZnCl2.
Comparisons of porous, surface chemistry and adsorption properties of carbon derived from Enteromorpha prolifera activated by H4P2O7 and KOH.
Journal of Physics and Chemistry of Solids, 74(6), 886-891. https://doi.org/10.1016/j.jpcs.2013.01.036 [22] Das, D., Samal, D.
Preparation, Surface and Pore Structure of High Surface Area Activated Carbon Fibers from Bamboo by Steam Activation.
Modification of the porous structure along the preparation of activated carbon monoliths with H3PO4 and ZnCl2.
Comparisons of porous, surface chemistry and adsorption properties of carbon derived from Enteromorpha prolifera activated by H4P2O7 and KOH.
Online since: February 2023
Authors: Shamo Tapdiqov, Maharat Huseynov, Fariz Ahmad, Sevda Kazimova
The filler composition leads to a better structuring of the gel.
One of the important parameters of study include the chemistry of the setting process during the solution injection into the wellbottom zone, the contact with porous rocks and the local environment conditions [9].
The reduction of permeability to the specified level when urea is added to the system is due to the interaction of the rock components used as a model with the silicate structure, continuous adhesion due to sickness and physicochemical forces [15].
Idris, H.Hamdan, Physiochemical and thermal properties of silica Aerogel–Poly vinyl alcohol/Core–Shell structure prepared using fluidized bed coating process for thermal insulation applications, Materials Chemistry and Physics, 215 (2018) 269-276
[17] N.Minju, N.N.Balagopal, S.Savithri, Sodium silicate-derived aerogels: effect of processing parameters on their applications, Royal Society of Chemistry, Advances, 11 (2021) 15301-15322
One of the important parameters of study include the chemistry of the setting process during the solution injection into the wellbottom zone, the contact with porous rocks and the local environment conditions [9].
The reduction of permeability to the specified level when urea is added to the system is due to the interaction of the rock components used as a model with the silicate structure, continuous adhesion due to sickness and physicochemical forces [15].
Idris, H.Hamdan, Physiochemical and thermal properties of silica Aerogel–Poly vinyl alcohol/Core–Shell structure prepared using fluidized bed coating process for thermal insulation applications, Materials Chemistry and Physics, 215 (2018) 269-276
[17] N.Minju, N.N.Balagopal, S.Savithri, Sodium silicate-derived aerogels: effect of processing parameters on their applications, Royal Society of Chemistry, Advances, 11 (2021) 15301-15322
Online since: August 2014
Authors: Dayang Habibah Abang Asmawi, Mazlina Mustafa Kamal
It is believed that the dispersion agent could coat the silica surfaces as they are being broken down during the mixing and then stabilize the dispersed structure by stearically preventing silica reagglomeration.
The additive could coat the silica surfaces as they are being broken down during the mixing and then stabilize the dispersed structure by stearically preventing silica reagglomeration5.
Figure 3 Figure 4 Figure 3 and Figure 4: Influence of mixing stage and additives on viscosity and dispersion in Epoxidised Natural Rubber compound Results showed that a three stage- mix can give an excellent dispersion owing to the high viscosity of two stage and this procedure can be recommended for dispersion of hard to disperse of filler low structure.
Hilton Rubber Chemistry and Technology: May 2002, Vol. 75, No. 2, pp. 215-245. (2002)
The additive could coat the silica surfaces as they are being broken down during the mixing and then stabilize the dispersed structure by stearically preventing silica reagglomeration5.
Figure 3 Figure 4 Figure 3 and Figure 4: Influence of mixing stage and additives on viscosity and dispersion in Epoxidised Natural Rubber compound Results showed that a three stage- mix can give an excellent dispersion owing to the high viscosity of two stage and this procedure can be recommended for dispersion of hard to disperse of filler low structure.
Hilton Rubber Chemistry and Technology: May 2002, Vol. 75, No. 2, pp. 215-245. (2002)
Online since: July 2022
Authors: Bo Zhao, Qiang Dai, Guang Hui Zhang, Meng He, Zhi Juan Zhao, Li Xian Wang
Study on Grain Boundary Sensitization in Heat Affected Zone of Austenitic Stainless Steel and Its Evaluation Method
Bo Zhao1,a, Qiang Dai1,b, Zhijuan Zhao1, c, Meng He1, d, Lixian Wang1,e,*, Guanghui Zhang2.f
1Institute of Chemistry, China Special Equipment Inspection and Research Institute,
Beijing, P.R.
In this paper, the simulated welding structure at different areas of heat affected zone (HAZ) of austenitic stainless steel are prepared by heating furnace, and the deference of intergranular corrosion resistance of all samples were determined by comparative methods of oxalic acid etching, hot-acid test and electrochemical potentiodynamic reactivation tests (EPR), and the effectiveness of all those methods were analysis and determination at the same time.
The result shows that the susceptibility degree at different areas of HAZ increased with the heating temperature increase, but all structures can pass hot-acid test and EPR test, indicating that it could maintain good performance of intergranular corrosion resistance.
Type of Structure Classified Types Microstructure in Microscope Heating Temperature 700℃ Dual Structure Some ditches occurring at grain boundaries but no grain being completely surrounded by a ditch. 800℃ Dual Structure Some ditches occurring at grain boundaries but no grain being completely surrounded by a ditch. 900℃ Step Structure No ditches found at grain boundaries. 1000℃ Step Structure No ditches found at grain boundaries. 1100℃ End-Grain Pitting I Structure contains a few deep end-grain pits along with some shallow etch pits 1200℃ End-Grain Pitting I Structure contains a few deep end-grain pits along with some shallow etch pits 1300℃ End-Grain Pitting I Structure contains a few deep end-grain pits along with some shallow etch pits Original Step Structure No ditches found at grain boundaries.
As shown in Table 2, the simulated microstructure of HAZ of austenitic stainless steel heated to 700-800 °C is classified as “Dual Structure”, indicating that the intergranular corrosion stabilization of austenitic stainless steel should be increased. when the heat treatment temperature rises above 1100 °C, it is obviously transformed to the “End-Grain Pitting I” of microstructure, indicating that there are obvious pits and the grain microstructures will be eroded.
In this paper, the simulated welding structure at different areas of heat affected zone (HAZ) of austenitic stainless steel are prepared by heating furnace, and the deference of intergranular corrosion resistance of all samples were determined by comparative methods of oxalic acid etching, hot-acid test and electrochemical potentiodynamic reactivation tests (EPR), and the effectiveness of all those methods were analysis and determination at the same time.
The result shows that the susceptibility degree at different areas of HAZ increased with the heating temperature increase, but all structures can pass hot-acid test and EPR test, indicating that it could maintain good performance of intergranular corrosion resistance.
Type of Structure Classified Types Microstructure in Microscope Heating Temperature 700℃ Dual Structure Some ditches occurring at grain boundaries but no grain being completely surrounded by a ditch. 800℃ Dual Structure Some ditches occurring at grain boundaries but no grain being completely surrounded by a ditch. 900℃ Step Structure No ditches found at grain boundaries. 1000℃ Step Structure No ditches found at grain boundaries. 1100℃ End-Grain Pitting I Structure contains a few deep end-grain pits along with some shallow etch pits 1200℃ End-Grain Pitting I Structure contains a few deep end-grain pits along with some shallow etch pits 1300℃ End-Grain Pitting I Structure contains a few deep end-grain pits along with some shallow etch pits Original Step Structure No ditches found at grain boundaries.
As shown in Table 2, the simulated microstructure of HAZ of austenitic stainless steel heated to 700-800 °C is classified as “Dual Structure”, indicating that the intergranular corrosion stabilization of austenitic stainless steel should be increased. when the heat treatment temperature rises above 1100 °C, it is obviously transformed to the “End-Grain Pitting I” of microstructure, indicating that there are obvious pits and the grain microstructures will be eroded.
Online since: October 2007
Authors: Sang Wook Woo, Kaoru Dokko, Kiyoshi Kanamura, Hiroyuki Nakano
A porous membrane of LiCoO2 with three dimensionally ordered macroporous
(3DOM) structure was obtained.
The prepared material had a rock-salt type crystallographic structure with mR3 space group.
LiCoO2 has a rock-salt type structure (space group: mR3 ), and Li+ ion can be inserted into the crystallographic structure reversibly at the electrode potential of 3.9 V vs.
Through this procedure, porous ceramic membrane with an inverse-opal structure was obtained.
Indeed, the 3D macroporous structure was collapsed at higher than 800 °C due to the grain growth.
The prepared material had a rock-salt type crystallographic structure with mR3 space group.
LiCoO2 has a rock-salt type structure (space group: mR3 ), and Li+ ion can be inserted into the crystallographic structure reversibly at the electrode potential of 3.9 V vs.
Through this procedure, porous ceramic membrane with an inverse-opal structure was obtained.
Indeed, the 3D macroporous structure was collapsed at higher than 800 °C due to the grain growth.
Online since: January 2010
Authors: Valentin Richter-Trummer, Pedro Miguel Guimarães Pires Moreira, Sérgio M.O. Tavares, Paulo Manuel Salgado Tavares de Castro
However, the application of new processes requires
taking into account effects that were not considered in riveted structures.
An integral structure can be obtained using welding processes, creating material continuity between the different parts, [6].
Another difference between welded and riveted structures is the residual stress field since the application of heat and sequential cooling creates internal stresses that may be beneficial or detrimental for the structure.
Boehm: New Engineering Processes in Aircraft Construction: Application of Laser-Beam and Friction Stir Welding; Glass Physics and Chemistry, Vol. 31, No. 1 (2005), pp. 27-29
Engle: Numerical analysis of crack propagation in cyclicloaded structures; Transactions of ASME, Journal of Basic Engineering, Vol. 89, (1967), pp. 459-464
An integral structure can be obtained using welding processes, creating material continuity between the different parts, [6].
Another difference between welded and riveted structures is the residual stress field since the application of heat and sequential cooling creates internal stresses that may be beneficial or detrimental for the structure.
Boehm: New Engineering Processes in Aircraft Construction: Application of Laser-Beam and Friction Stir Welding; Glass Physics and Chemistry, Vol. 31, No. 1 (2005), pp. 27-29
Engle: Numerical analysis of crack propagation in cyclicloaded structures; Transactions of ASME, Journal of Basic Engineering, Vol. 89, (1967), pp. 459-464
Online since: April 2018
Authors: Lin Zhang, Juan Xia, Qi Wang
Synthesis and Photocatalytic Properties of the Bi2MoO6 and Bi2WO6 Photocatalysts
Juan Xiaa*, Lin Zhangb and Qi Wangc
School of Chemistry and Chemical Engineering, Fuyang Normal College, Fuyang Anhui 236037, China
axj871009@163.com, b715zhanglin@163.com, c694152316@qq.com
Keywords: photocatalytic; bismuth molybdate; bismuth tungstate; hydrothermal;
Abstract.
Results and Discussion Fig. 1 depicts the crystallographic structure and phase purity of the obtained samples by X-ray diffraction (XRD) patterns.
Figs. 2a and c. show the undistorted panoramic view of the Bi2MoO6 andBi2WO6 materials, which consisting of nanowire and nanoplate structures respectively.
However, the detailed structure of the Bi2WO6 material shows the nanoplate with a thickness of approximately 10 nm and a width of 100 nm.
Wang, J.Chen, Formation, structure and physical properties of a series of a-MoO3nanocrystals: from 3D to 1D and 2D, CrystEngComm, 14 (2012) 2675-2682
Results and Discussion Fig. 1 depicts the crystallographic structure and phase purity of the obtained samples by X-ray diffraction (XRD) patterns.
Figs. 2a and c. show the undistorted panoramic view of the Bi2MoO6 andBi2WO6 materials, which consisting of nanowire and nanoplate structures respectively.
However, the detailed structure of the Bi2WO6 material shows the nanoplate with a thickness of approximately 10 nm and a width of 100 nm.
Wang, J.Chen, Formation, structure and physical properties of a series of a-MoO3nanocrystals: from 3D to 1D and 2D, CrystEngComm, 14 (2012) 2675-2682
Online since: September 2005
Authors: Manuel E. Brito, Teruhisa Horita, Katsuhiko Yamaji, Natsuko Sakai, Harumi Yokokawa, Yue Ping Xiong, Haruo Kishimoto
Therefore, the relationship between defect chemistry and cathodic polarization should be
clarified at the cathode/electrolyte ceramic interfaces.
] (10) where, C indicates the concentration of oxygen in the lattice, which is assumed to be unity. f is the correlation factor, which is determined by the crystal structure (in this case set as 0.65). γ is the thermodynamic enhancement factor.
The SIMS depth profiles of cations suggest the layered structure in the oxide scale and alloy inside.
Solid State Chemistry, 93, 212 (1991). 6.
Solid State Chemistry, 123, 382 (1996). 20.
] (10) where, C indicates the concentration of oxygen in the lattice, which is assumed to be unity. f is the correlation factor, which is determined by the crystal structure (in this case set as 0.65). γ is the thermodynamic enhancement factor.
The SIMS depth profiles of cations suggest the layered structure in the oxide scale and alloy inside.
Solid State Chemistry, 93, 212 (1991). 6.
Solid State Chemistry, 123, 382 (1996). 20.
Online since: November 2013
Authors: Yi Min Zhu, Yan Ping Yang, Wen Dan Wang, Yan Feng Li, Duo Zhen Ren, Zhi Dong Tang
In addition, the relationship between floatability of DXS and crystal structure of cassiterite was investigated.
The effect of mineral crystal structure to the flotability.
The structure is shown in Figure 5(a).The tin-oxide bond has changed from covalent to ionic.
Therefore the bond Si4+-O2- is stronger than Sn4+-O2-, and is harder to break in the mineral crystal structure.
Flotation Chemistry for Cassitetite [J].
The effect of mineral crystal structure to the flotability.
The structure is shown in Figure 5(a).The tin-oxide bond has changed from covalent to ionic.
Therefore the bond Si4+-O2- is stronger than Sn4+-O2-, and is harder to break in the mineral crystal structure.
Flotation Chemistry for Cassitetite [J].
Online since: January 2013
Authors: Jin Juan Hu, Yi Ding Shen, Hai Hua Wang, Juan Zhang, Gui Qiang Fei
Preparation and properties of waterborne cationic polyurethanes/polypyrrole conductive composites
Haihua Wang*, Jinjuan Hu, Yiding Shen, Guiqiang Fei,Juan zhang
Key laboratory of Auxiliary Chemistry & Technology for Chemical Industry, Ministry of Education.
The structure, morphology and thermal stability were also characterized by Fourier infrared spectra (FT-IR), light scattering, TEM, and TGA.
Simultaneously the structure, morphology, thermal stability, electrical conductivity, and conductivity stability of conductive composites were investigated by various analytical techniques.
The structure, morphology and thermal stability were also characterized by Fourier infrared spectra (FT-IR), light scattering, TEM, and TGA.
Simultaneously the structure, morphology, thermal stability, electrical conductivity, and conductivity stability of conductive composites were investigated by various analytical techniques.