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Online since: July 2016
Authors: Gheorghe Nagit, Mihai Boca, Laurentiu Slatineanu
He also identified in such conditions some fine-grain structures, which can improve a uniform-elongation of the nugget.
Table 2: Welding parameters and the nuggets diameters Sample number Current value, [kA] Force value, [kN] Time per welding (soft cycle), [s] Holding time [s] Nugget diameter (Dn), [mm] 1 5 4 0.7 2 5.1 2 5.1 3 4.9 4 4.8 5 4.9 6 5.0 7 4.9 8 4.9 9 5.0 10 4.9 Figure 4: Image of the mark obtained by means of the AFFRI equipment (magnification: 10x) In order to determine the micro hardness of the welded parts, it was necessary to obtain flat surfaces; the test samples were sectioned along the axis of the welded nugget using a disc tool and adequate cutting equipment.
Subsequently, the resulted surfaces were finished by abrasion using silicon carbide with low grain sizes.
Analysing the hardness map, it can say that sometimes there are large gaps between measured values of distinct interest areas which could be caused by inhomogeneity and changes in the grain size of the materials in the newly formed structures.
Table 2: Welding parameters and the nuggets diameters Sample number Current value, [kA] Force value, [kN] Time per welding (soft cycle), [s] Holding time [s] Nugget diameter (Dn), [mm] 1 5 4 0.7 2 5.1 2 5.1 3 4.9 4 4.8 5 4.9 6 5.0 7 4.9 8 4.9 9 5.0 10 4.9 Figure 4: Image of the mark obtained by means of the AFFRI equipment (magnification: 10x) In order to determine the micro hardness of the welded parts, it was necessary to obtain flat surfaces; the test samples were sectioned along the axis of the welded nugget using a disc tool and adequate cutting equipment.
Subsequently, the resulted surfaces were finished by abrasion using silicon carbide with low grain sizes.
Analysing the hardness map, it can say that sometimes there are large gaps between measured values of distinct interest areas which could be caused by inhomogeneity and changes in the grain size of the materials in the newly formed structures.
Online since: January 2009
Authors: Chun Yao Zhan, Wei Wang, Zhen Lei Tang, Zuo-Ren Nie
Nie et.al found that Er in
alloy can play an important role like that of Sc and Zr, which could optimize grain structure, and
improve comprehensive mechanical properties, thermal stability and weldability.
We also predict that interaction energy of Al-Er is much negative under the same temperature, which showed that bonding ability and interaction of Al and Er is stronger, and they have a great tendency to combine in alloy solution, the composition super-cooling in the interface occurred easily during the solidification, naturally prone to segregate, even though the concentration of Er is small, the Al3Er phase precipitate preferential at interface, which act as the center of heterogeneity nucleus, naturally remarkable refine grain size.
Conclusion 1)Er concentration in Al-Er alloy shows a negative deviation from Rault's Law at 1073K, deviation degree is larger at the low concentration range, therefore real concentration is low, mainly due to Er atoms are prone to segregate at interface or dislocation; 2)The interaction parameters between Al and Er is LAl-Er=-204.29exp(-T/2000) kJ/mol, which shows the bonding ability and interaction energy between Al and Er are strong, and Al and Er have a great tendency to combine in alloy solution, the composition super-cooling in the interface occurs easily during the solidification, intensively refine grain size; 3)The minimum of mixing enthalpy, excess Gibbs energy and excess entropy are -38.5 kJ /mol, -27.6kJ/mol, -10.5J/mol respectively in the whole concentration range, which indicate that properties of alloy solution are stable.
Acknowledgement The authors thank the financial supports of the State Key Foundamental Research Project of China with the contract number (2005CB 623706) and China National Outstanding Youth Plan (50525413) and Beijing Education Plan (KM200710005011 and 000855).
We also predict that interaction energy of Al-Er is much negative under the same temperature, which showed that bonding ability and interaction of Al and Er is stronger, and they have a great tendency to combine in alloy solution, the composition super-cooling in the interface occurred easily during the solidification, naturally prone to segregate, even though the concentration of Er is small, the Al3Er phase precipitate preferential at interface, which act as the center of heterogeneity nucleus, naturally remarkable refine grain size.
Conclusion 1)Er concentration in Al-Er alloy shows a negative deviation from Rault's Law at 1073K, deviation degree is larger at the low concentration range, therefore real concentration is low, mainly due to Er atoms are prone to segregate at interface or dislocation; 2)The interaction parameters between Al and Er is LAl-Er=-204.29exp(-T/2000) kJ/mol, which shows the bonding ability and interaction energy between Al and Er are strong, and Al and Er have a great tendency to combine in alloy solution, the composition super-cooling in the interface occurs easily during the solidification, intensively refine grain size; 3)The minimum of mixing enthalpy, excess Gibbs energy and excess entropy are -38.5 kJ /mol, -27.6kJ/mol, -10.5J/mol respectively in the whole concentration range, which indicate that properties of alloy solution are stable.
Acknowledgement The authors thank the financial supports of the State Key Foundamental Research Project of China with the contract number (2005CB 623706) and China National Outstanding Youth Plan (50525413) and Beijing Education Plan (KM200710005011 and 000855).
Online since: June 2012
Authors: Lei Yu, Jin Xi Zhang, Kai Mu
The tests conducted on specimens and the numbers and dimensions of each kind of specimens produced in this study are different with each other.
Obviously, the size and shape of IOT grains are smaller and more irregular respectively than those of NS ones.
Comparing to mortars with NS as fine aggregate, those with IOT as fine aggregate, the size and shape of IOT grains are both finer and more irregular respectively. 2.
In summary, comparing to reference sand, as fine aggregate, iron ore tailings can enhance compressive strength related to its finer and more irregular grain shape and the ability on complicating porous structure in mortars.
Obviously, the size and shape of IOT grains are smaller and more irregular respectively than those of NS ones.
Comparing to mortars with NS as fine aggregate, those with IOT as fine aggregate, the size and shape of IOT grains are both finer and more irregular respectively. 2.
In summary, comparing to reference sand, as fine aggregate, iron ore tailings can enhance compressive strength related to its finer and more irregular grain shape and the ability on complicating porous structure in mortars.
Online since: February 2016
Authors: Victor I. Sachkov, Larisa Sotnikova, Alexander Vladimirov, Anton Stepanov, Sergey Sozinov, Fiodor Titov, Anna N. Popova
Therefore, recently improved efficiency of TiO2 based photocatalysts is associated with the synthesis of the anatase crystalline particles containing a greater number of unstable faces (001) [5-6], or thermodynamically less stable TiO2 modifications, such as brookite [6-7].
Thus, having been heated to 300°С in vacuum and in air, TiO2 film structure can be represented as an amorphous matrix with separate anatase crystal grains.
Temperature increase to 400°С leads to increase of existing anatase crystal grains and formation of new rutile crystal grains in TiO2 films, but does not transform it into crystalline state.
Thus, having been heated to 300°С in vacuum and in air, TiO2 film structure can be represented as an amorphous matrix with separate anatase crystal grains.
Temperature increase to 400°С leads to increase of existing anatase crystal grains and formation of new rutile crystal grains in TiO2 films, but does not transform it into crystalline state.
Online since: October 2010
Authors: Pei Hao Li, Wen Jun Qu
Materials and Methods
Bacterial Strain and Culture Media The microorganism used throughout the study was
Sporosarcina pasteurii (strain number 11859 provided by American Type Culture
Collection(ATCC)).The diameter of rotundity spore is about 0.5~1.5μm.
However, samples subjected to bacterially induced mineralization showed much less damage, and the newly formed carbonate grains were not removed in detectable amounts.
However, samples subjected to bacterially induced mineralization showed much less damage, and the deposit grains were not removed in detectable amounts(Fig. 5, Fig. 6).
SEM observations and weight loss measurements of sonicated samples demonstrate the strong adhesion between the samples and the deposit grains, as well as the positive consolidating and/or protecting effect of the biodeposition. 0 5 10 15 20 25 30 0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1.0 1.1 1.2 1.3 1.4 1.5 1.6 1.7 1.8 1.9 2.0 a △Wt / % Time / min culture sonicated control sonicated uninoculation sonicated fresh sonicated culture non-sonicated control non-sonicated fresh non-sonicated 0 5 10 15 20 25 30 0.00 0.05 0.10 0.15 0.20 0.25 0.30 0.35 0.40 0.45 0.50 0.55 0.60 b △Wt / % Time / min culture sonicated control sonicated uninoculation sonicated fresh sonicated culture non-sonicated control non-sonicated fresh non-sonicated (a) Concrete (Urea-CaCl2) (b) Marble (Urea-CaCl2) Figure 8: Mass loss (△W) vs ultrasonication time of samples Conclusionss Bacterially induced mineralization
However, samples subjected to bacterially induced mineralization showed much less damage, and the newly formed carbonate grains were not removed in detectable amounts.
However, samples subjected to bacterially induced mineralization showed much less damage, and the deposit grains were not removed in detectable amounts(Fig. 5, Fig. 6).
SEM observations and weight loss measurements of sonicated samples demonstrate the strong adhesion between the samples and the deposit grains, as well as the positive consolidating and/or protecting effect of the biodeposition. 0 5 10 15 20 25 30 0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1.0 1.1 1.2 1.3 1.4 1.5 1.6 1.7 1.8 1.9 2.0 a △Wt / % Time / min culture sonicated control sonicated uninoculation sonicated fresh sonicated culture non-sonicated control non-sonicated fresh non-sonicated 0 5 10 15 20 25 30 0.00 0.05 0.10 0.15 0.20 0.25 0.30 0.35 0.40 0.45 0.50 0.55 0.60 b △Wt / % Time / min culture sonicated control sonicated uninoculation sonicated fresh sonicated culture non-sonicated control non-sonicated fresh non-sonicated (a) Concrete (Urea-CaCl2) (b) Marble (Urea-CaCl2) Figure 8: Mass loss (△W) vs ultrasonication time of samples Conclusionss Bacterially induced mineralization
Online since: May 2015
Authors: František Hnilica, Jaroslav Malek, Jaroslav Veselý
Introduction
The prolonged life-expectancy leads to an increasing number of people that require the replacements of degenerated or damaged tissues by artificial materials.
In all studied cold swaged (with minimal section reduction 75%) and solution treated specimens the microstructure consists of equiaxed β-grains (see Fig. 6).
During aging treatment (450°C/8h/water quenched) of cold swaged (section reduction 90%) specimen with the lowest oxygen content fine needle-like α-particles precipitated in grain interiors.
There can be also observed coarser precipitates on grain boundaries, which can be also distinguished in light micrographs (Fig. 7a,b).
In all studied cold swaged (with minimal section reduction 75%) and solution treated specimens the microstructure consists of equiaxed β-grains (see Fig. 6).
During aging treatment (450°C/8h/water quenched) of cold swaged (section reduction 90%) specimen with the lowest oxygen content fine needle-like α-particles precipitated in grain interiors.
There can be also observed coarser precipitates on grain boundaries, which can be also distinguished in light micrographs (Fig. 7a,b).
Online since: January 2013
Authors: Yue Qin Liu, Man Quan Zhao, Yong Wen Hu
Standard k-ε turbulence model of turbulent kinetic energy equation
(3)
Standard k-ε turbulence model dissipation rate equation
(4)
In (3) and (4), k-turbulence kinetic energy; μt is turbulent viscosity, Pa/s; σk, σε is turbulent Schmidt number of the k equation and ε equation; C1ε is turbulent kinetic energy of the shear rate multipliers; C2ε is turbulent kinetic energy dissipation of the multiplier; Cμ is turbulent viscosity correction factor; the C3 is k-ε buoyancy model coefficients; C4 is k-ε buoyancy multiplier; β is coefficient of thermal expansion; σt is empirical parameters; T is Temperature, k; Ф is viscous heat generated items.
(5) Where, Hcmax is vacuum maximum value of the vacuum chamber, kPa; d is suction hole diameter of the seed plate, cm; C is distance between the center of seed gravity and the suction seed plate, cm; m is one seed quality, kg; v is line speed at the center of the suction hole on the row seed plate, m/s; r is turning radius at the suction hole of the row seed plate, m; g is acceleration due to gravity, m/s2; λ is seed frictional resistance combined factor, λ=(6 to 10) tan θ, θ is natural angle of repose of the seed; K1 is coefficient of reliability of the absorption seed, taking 1.8 to 2.0, thousand grain weight of the seed are small and shape spherical, taking a small value; K2 is outsidecondition factor, taking 1.6 to 2.0, it take greater when the seed grain weight is large.
The test used the seed plate with diameter of 180 mm and thickness of 2 mm, according to the literature[14], the suction hole diameter selected 4.2 mm for small grain corn. 1. rack 2.exciter 3. sediment device 4. pulley 5. sandbox 6. triangle bracket 7. seed containers 8. air-suction seed metering device 9. the inverter 10. conveyor belt 11. fan 12. exciter control panel Fig.5 The simulated surface air-suction seed metering test-bed Experimental analysis of rowing performance of different distribution diameter of suction hole.
(5) Where, Hcmax is vacuum maximum value of the vacuum chamber, kPa; d is suction hole diameter of the seed plate, cm; C is distance between the center of seed gravity and the suction seed plate, cm; m is one seed quality, kg; v is line speed at the center of the suction hole on the row seed plate, m/s; r is turning radius at the suction hole of the row seed plate, m; g is acceleration due to gravity, m/s2; λ is seed frictional resistance combined factor, λ=(6 to 10) tan θ, θ is natural angle of repose of the seed; K1 is coefficient of reliability of the absorption seed, taking 1.8 to 2.0, thousand grain weight of the seed are small and shape spherical, taking a small value; K2 is outsidecondition factor, taking 1.6 to 2.0, it take greater when the seed grain weight is large.
The test used the seed plate with diameter of 180 mm and thickness of 2 mm, according to the literature[14], the suction hole diameter selected 4.2 mm for small grain corn. 1. rack 2.exciter 3. sediment device 4. pulley 5. sandbox 6. triangle bracket 7. seed containers 8. air-suction seed metering device 9. the inverter 10. conveyor belt 11. fan 12. exciter control panel Fig.5 The simulated surface air-suction seed metering test-bed Experimental analysis of rowing performance of different distribution diameter of suction hole.
Online since: October 2016
Authors: Ji Ling Feng, Shi Wen Wang, Jian Guo Lin
N is the total number of slip systems.
The hardening is contributed by dislocations at both global and local slip systems levels within a grain.
Lin, et al, Three-dimensional virtual grain structure generation with grain size control, Mech.
The hardening is contributed by dislocations at both global and local slip systems levels within a grain.
Lin, et al, Three-dimensional virtual grain structure generation with grain size control, Mech.
Online since: August 2004
Authors: Bernard Pieraggi, Didier Adé, Yannick Le Maoult
After compaction and thermomechanical processing, the alloy is recrystallised to generate a coarse
microstructure showing high grain aspect ratio to avoid as much as possible that the creep resistance
be impaired by grain boundary sliding or the formation of grain boundary creep pores.
Therefore, an estimate of εc can be obtained directly from only the measurement of height h of a larger number of trajectories.
Therefore, an estimate of εc can be obtained directly from only the measurement of height h of a larger number of trajectories.
Online since: September 2013
Authors: Shu Zhong Wang, Xiao Sun, Xiang Rong Luo, Xiao Juan Ren
Mainly because the sand ratio increases to a certain extent, proppant grain distribution is dense, the reunion phenomenon occurred in a fracturing fluid,and fracturing fluid viscosity makes the dense sand particles group act like a big particles, equivalent to greatly increase the particle diameter, causing particle settling velocity increase.This phenomenon is also referred to as "particle reunion" effect.
3.4 correlations for critical sedimentation velocity and particle settling velocity
Through the analysis of the above experimental results, considering the influences of sand ratio, temperature and foam quality on proppant settling velocity and critical settling velocity of fracturing fluid, the type(1) and (2) are fitting results to show correlations form calculated the particle settling velocity ut and critical settling velocity Vcr of fracturing fluid, the average error are 12.32% and 13.5% respectively:
The proppant grain density is about 1700 kg·m-3. the type scope of application is: 0≤CS≤10%, 10%≤Г≤85%, 40℃≤T≤80℃, P=10MPa
Conclusion 1)The proppant transport experimental results show that with increase of the temperature, the proppant grain in GRF-CO2 foam fracturing fluid sedimentation rate increases,at the same time, the fracturing fluid critical settling velocity increase, showing the proppant transport performance degradation. 2)Under the condition of foaming, with increase of the foam quality, proppant particle settling velocity reduces, fracturing fluid critical settling velocity reduces, proppant transport performance increases;The change law under not foaming condition is just the opposite.
:“Thermophysical Properties of Fluid Systems” in MIST Chemistry WebBook, NIST Standard Reference DataBase Number 69, Eds.
The proppant grain density is about 1700 kg·m-3. the type scope of application is: 0≤CS≤10%, 10%≤Г≤85%, 40℃≤T≤80℃, P=10MPa
Conclusion 1)The proppant transport experimental results show that with increase of the temperature, the proppant grain in GRF-CO2 foam fracturing fluid sedimentation rate increases,at the same time, the fracturing fluid critical settling velocity increase, showing the proppant transport performance degradation. 2)Under the condition of foaming, with increase of the foam quality, proppant particle settling velocity reduces, fracturing fluid critical settling velocity reduces, proppant transport performance increases;The change law under not foaming condition is just the opposite.
:“Thermophysical Properties of Fluid Systems” in MIST Chemistry WebBook, NIST Standard Reference DataBase Number 69, Eds.