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Online since: September 2013
Authors: Olurotimi A. Dahunsi, Temidayo Oluwagbenga Johnson, Olayinka O. Awopetu
Diffraction data for pure phases, obtained from the International Centre for Diffraction Data (ICDD) database using JCPDS cards, was used to identify what phases were present in the material.
Patent Number 4390365, U.S.
Patent Number 4390365, U.S.
Online since: July 2011
Authors: Ranna Tolouei, Wan Dung Teng, Chou Yong Tan, Singh Ramesh, Mahdi Amiriyan, Iis Sopyan
Bone and joint diseases account for half of all chronic conditions in people over 50 years of age and the number of people suffering from this diseases are expected to increase steeply around the globe by year 2020 [2].
The XRD analysis of synthesized HA powder as well as sintered HA samples shown in Fig. 2, indicates peaks that correspond to the standard JCPDS card no: 74-566 for stoichiometric HA.
The XRD analysis of synthesized HA powder as well as sintered HA samples shown in Fig. 2, indicates peaks that correspond to the standard JCPDS card no: 74-566 for stoichiometric HA.
Online since: February 2009
Authors: Dinesh Amalnerkar, Ranjit R. Hawaldar, Uttam Mulik, Sujata Waghmare, Manish Shinde, Ramkrishna Gholap, N. Koteswara Rao
Quite notably, the diffractograms corresponding to heated admixtures of AgNO3:PPS (all
molar ratios) clearly evince predominance of mainly metallic silver as can be indexed by prominent
diffraction peaks at d values of 2.33, 2.02, 1.43 and 1.22 Å (cubic phase, JCPDS Card No. 040783).
(ii) Nevertheless, XRD corresponding to heated admixture of AgNO3 and PPS when taken in equimolar ratio reveals formation of acanthite Ag2S which can be judged by characteristic diffraction peaks at d values of 3.07, 2.83, 2.65, 2.59, 2.43, 2.21, and 2.07 Å (monoclinic phase, JCPDS Card No. 14-0072).
The number of spots in their SAED patterns evidences the single crystalline nature of such nanoparticles.
(ii) Nevertheless, XRD corresponding to heated admixture of AgNO3 and PPS when taken in equimolar ratio reveals formation of acanthite Ag2S which can be judged by characteristic diffraction peaks at d values of 3.07, 2.83, 2.65, 2.59, 2.43, 2.21, and 2.07 Å (monoclinic phase, JCPDS Card No. 14-0072).
The number of spots in their SAED patterns evidences the single crystalline nature of such nanoparticles.
Online since: April 2016
Authors: Serge Zhuiykov
All reflections were indexed to orthorhombic β-WO3 phase (JCPDS card No. 20-1324 with space group P and the following lattice parameters: a = 7.384Å, b = 7.512Å, c = 3.864Å).
This shift indicates the contribution of W5+-states from non-stoichiometric oxide phase of WO3-x in comparison with stoichiometric WO3 owing to the increased number of oxygen vacancies created during the intercalation.
This shift indicates the contribution of W5+-states from non-stoichiometric oxide phase of WO3-x in comparison with stoichiometric WO3 owing to the increased number of oxygen vacancies created during the intercalation.
Online since: October 2002
Authors: Regina da Conceição Corredeira Monteiro, M.C. Ferro, Christian Leroy, Maria Helena F.V. Fernandes
If the
vitrification process is followed by adequate thermal treatments, it is possible to obtain glassceramics
with chemical and physical properties suitable for a number of different applications as
cladding materials (e.g. kitchen and laboratory benches, cooker plates, walls, roofs, floors) [4-6].
(JCPDS file card no. is indicated) 10 20 30 40 50 60 70 2� (degree) Intensity (au) GC-800 GC-870 40-496 Esseneite (7) 35-424 Nepheline (9) SEM micrographs, Figure 2, show that bulk crystallization occurred at both temperatures, giving rise to quite homogeneous fine-grained microstructures.
(JCPDS file card no. is indicated) 10 20 30 40 50 60 70 2� (degree) Intensity (au) GC-800 GC-870 40-496 Esseneite (7) 35-424 Nepheline (9) SEM micrographs, Figure 2, show that bulk crystallization occurred at both temperatures, giving rise to quite homogeneous fine-grained microstructures.
Online since: April 2007
Authors: Jun Zhou, Yan Xin Wang
The XRD patterns of CG-GCs and GG-GCs (Fig.2)
show that the reflections of both are similar, and are in
agreement with those of β-wollastonite in JCPDS card,
which signifies that cracked-glass panels and glass
grains can equally deposit β-wollastonite crystals.
The 1 000 multiple micrograph (Fig.3a) shows that the CG-GCs are composed of pine-like druses and residual glass phase, while the 10 000 multiple micrograph (Fig.3b) further reveals that the pine-like druses are piled by a number of granular crystals with the size ranging from 0.2µm to 0.5µm.
The 1 000 multiple micrograph (Fig.3a) shows that the CG-GCs are composed of pine-like druses and residual glass phase, while the 10 000 multiple micrograph (Fig.3b) further reveals that the pine-like druses are piled by a number of granular crystals with the size ranging from 0.2µm to 0.5µm.
Online since: June 2014
Authors: Ze Jun Chen, La Yun Deng, Hong Chen, You Hua Fan
The main five diffraction peaks were identified to match up to the (110), () and (111), () and (020) planes of the monoclinic CuO structure in sequence compared with the PDF card (JCPDS 45-0937).
When the initial concentration was 0.075 M, in addition to generate a large number of carambola-shaped particle with the size of 200-300 nm, there also randomly appeared square shaped CuO particles on the copper wafer substrate.
When the initial concentration was 0.075 M, in addition to generate a large number of carambola-shaped particle with the size of 200-300 nm, there also randomly appeared square shaped CuO particles on the copper wafer substrate.
Online since: April 2016
Authors: Bin Song Wang, Jie Zhang, Ying Zhang, Maria Shishova
It is closely matched with the reported reference values of International Centre for Diffraction Data (ICDD) card number (JCPDS File No.: 01-1167)[12] and suggested that biogenic Ag NPs are highly crystalline in nature and indicated that Ag+ had been reduced to Ag(0) by the bacteria.
Online since: May 2016
Authors: W. Rahman, Uda Hashim, Abdul Rahman Nurul Huda, Hon Cheun Lee, Suhaimi Mat Kahar, Kai Loong Foo, Puah Ying Phing Adelyn, Wei Wen Liu, Chang Chuan Lee, Bee Ying Lim, Mohd Khairuddin Md Arshad, Chun Hong Voon, A. Rahim Ruslinda
Three peaks that were corresponded to ß-SiC, with (111), (220) and (311) crystal planes of cubic ß-SiC (JCPDS card 074-2307) with 2θ of 36˚ , 61˚ and 72.5˚were observed.
Acknowledgements This work was financially supported by the Department of Higher Education, Ministry of Higher Education, (KPT) through the Fundamental Research Grant Scheme (FRGS) with the grant number 9003-00441.
Acknowledgements This work was financially supported by the Department of Higher Education, Ministry of Higher Education, (KPT) through the Fundamental Research Grant Scheme (FRGS) with the grant number 9003-00441.