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Online since: July 2025
Authors: Atia Balkis, Riski Dwimalida Putri, Dori Fitria
Research Methods
Materials
The equipment used includes magnetic stirrers, hot plates, analytical balances, ultraviolet lamps, needles, autoclaves, ovens, bunsen lamps, and glassware.
The materials used were cinnamaldehyde (Merck), 2-acetylnaphthalene (Sigma Aldrich), KOH, ethanol (Supelco), ethyl acetate (Supelco), n-hexane (Supelco), GF254 TLC plate (Merck), nutrient agar (NA), nutrient broth (NB), aqua dest, 70% ethanol, Escherichia coli, and Staphylococcus aureus bacteria.
Until the product is obtained, TLC is then carried out, by highlighting the starting materials, namely cinnamaldehyde and 2-acetylnaphthalene, as well as the product.
One of the syntheses was carried out using the starting materials cinnamaldehyde and 2-acetylnaphthalene but using a NaOH base catalyst and obtained a yield of 65-83%.
The Cinnamylideneacetophenone compound was synthesized using the starting materials cinnamaldehyde and 2-acetylnaphthalene, using a KOH base catalyst in ethanol/distilled water (50% v/v) at room temperature for 24 hours.
The materials used were cinnamaldehyde (Merck), 2-acetylnaphthalene (Sigma Aldrich), KOH, ethanol (Supelco), ethyl acetate (Supelco), n-hexane (Supelco), GF254 TLC plate (Merck), nutrient agar (NA), nutrient broth (NB), aqua dest, 70% ethanol, Escherichia coli, and Staphylococcus aureus bacteria.
Until the product is obtained, TLC is then carried out, by highlighting the starting materials, namely cinnamaldehyde and 2-acetylnaphthalene, as well as the product.
One of the syntheses was carried out using the starting materials cinnamaldehyde and 2-acetylnaphthalene but using a NaOH base catalyst and obtained a yield of 65-83%.
The Cinnamylideneacetophenone compound was synthesized using the starting materials cinnamaldehyde and 2-acetylnaphthalene, using a KOH base catalyst in ethanol/distilled water (50% v/v) at room temperature for 24 hours.
Online since: November 2005
Authors: Jiri Kliber, Bohuslav Mašek, Ondrej Zacek, H. Staňková
Stankova
2,d
1
Department of Materials Forming, Faculty of Metallurgy and Materials Engineering, VSBTechnical
University of Ostrava, Czech Republic
2
Department of Material Science and Technology, Faculty of Mechanical Engineering, University
of West Bohemia in Pilsen, Czech Republic
a
jiri.kliber@vsb.cz, b
ondrej.zacek@vsb.cz, c masekb@kmm.zcu.cz, dhstankov@kmm.zcu.cz
Keywords: Transformation induced plasticity, carbon steel with Si, retained austenite, annealing,
hot forming
Abstract.
The present paper thus involves study of the austenitization temperature effects and holding times at these temperatures with subsequent forming of materials, straining in intercritical region and rapid cooling down to the area of bainite nose and holding at this temperature.
The objective of this paper is to identify optimum forming conditions with subsequent controlled cooling or optimum conditions of separate heat treatment to achieve a high ductility of materials.
Meyer: International Journal of Plasticity Vol.16 (2000), p. 1391
Kliber: 12 th International Metallurgical and Materials conference "METAL 2002".
The present paper thus involves study of the austenitization temperature effects and holding times at these temperatures with subsequent forming of materials, straining in intercritical region and rapid cooling down to the area of bainite nose and holding at this temperature.
The objective of this paper is to identify optimum forming conditions with subsequent controlled cooling or optimum conditions of separate heat treatment to achieve a high ductility of materials.
Meyer: International Journal of Plasticity Vol.16 (2000), p. 1391
Kliber: 12 th International Metallurgical and Materials conference "METAL 2002".
Online since: July 2011
Authors: M. Mascot, J.C. Carru, Didier Fasquelle
The optimized annealing conditions (950°C for 15 min) give the following results: εr = 780 and tgδ = 0.01 at 100 kHz, Pr = 13 µC/cm², Ec = 63 kV/cm and a tunability of 55%.
1 Introduction
Piezoelectric actuators, infrared sensors, FeRAM usually contain lead based materials [1-2].
Among these materials, PbZrTiO3 (PZT) is the most used thanks to its superior piezoelectric performances.
Accordingly, it is now necessary to implement materials without prohibited substances.
[5] Alexandru H.V, Berbecaru C, Ioachim A,Banciu M.G, Toacsen M.I, Nedelcu L, Ghetu D, Stoica G, Materials Science and Engineering B118 (2005) 92-96
[8] Malic B, Boerasu I, Mandeljc M, Kosec M, Sherman V, Yamada T, Setter N, Vakadinovic M, Journal of European Ceramic Society 27 (2007) 2945-2948
Among these materials, PbZrTiO3 (PZT) is the most used thanks to its superior piezoelectric performances.
Accordingly, it is now necessary to implement materials without prohibited substances.
[5] Alexandru H.V, Berbecaru C, Ioachim A,Banciu M.G, Toacsen M.I, Nedelcu L, Ghetu D, Stoica G, Materials Science and Engineering B118 (2005) 92-96
[8] Malic B, Boerasu I, Mandeljc M, Kosec M, Sherman V, Yamada T, Setter N, Vakadinovic M, Journal of European Ceramic Society 27 (2007) 2945-2948
Online since: May 2015
Authors: Andrzej Sioma
Context Transformations of Range Images Using Directional
Data Back Fill Algorithm
Andrzej Sioma1,a
1AGH University of Science and Technology, Faculty of Mechanical Engineering and Robotics, Al.
Comparison of the final results of the measurement and boundary values provides grounds for the surface quality control as well as for decisions concerning potential qualification of the material as a reject.
References [1] Bednarczyk J., Sioma A. (2011), “Application of a visual measurement technique to the assessment of electrodynamic stamping”, Solid State Phenomena ; Control engineering in materials processing, ISSN 1012-0394, vol.177, pp. 1–9, 20
[6] Kowal J., Karwat B., Sioma A.(2012): Using three-dimensional images in the description of environment and biological structures, Polish Journal of Environmental Studies ; ISSN 1230-1485. 2012 vol. 21 no. 5A s. 227–232.
[8] Tytko A., Sioma A. (2011): “Evaluation of the operational parameters of ropes”, Solid State Phenomena, Control engineering in materials processing, ISSN 1012-0394, vol.177, pp. 125–134
Comparison of the final results of the measurement and boundary values provides grounds for the surface quality control as well as for decisions concerning potential qualification of the material as a reject.
References [1] Bednarczyk J., Sioma A. (2011), “Application of a visual measurement technique to the assessment of electrodynamic stamping”, Solid State Phenomena ; Control engineering in materials processing, ISSN 1012-0394, vol.177, pp. 1–9, 20
[6] Kowal J., Karwat B., Sioma A.(2012): Using three-dimensional images in the description of environment and biological structures, Polish Journal of Environmental Studies ; ISSN 1230-1485. 2012 vol. 21 no. 5A s. 227–232.
[8] Tytko A., Sioma A. (2011): “Evaluation of the operational parameters of ropes”, Solid State Phenomena, Control engineering in materials processing, ISSN 1012-0394, vol.177, pp. 125–134
Online since: July 2009
Authors: Lyudmila N. Paritskaya, V.V. Bogdanov, Yuri S. Kaganovsky
Bogdanov2c
1
Resnick Institute for Advanced Technology, Department of Physics, Bar-Ilan University,
Ramat-Gan 52900, Israel;
2
Department of Crystal Physics, Karazin Kharkov National University, Kharkov 61077,
Ukraine
a
kagany@mail.biu.ac.il,
b
lparitskaya@hotmail.com, cbogdanov@univer.kharkov.ua
submitted: 9 July 2008 revised: 15 December 2008 accepted: 15 December 2008
Keywords: Cu-Sn thin films, reactive grain boundary interdiffusion, intermetallic phases,
lateral phase propagation, nano-materials, grain boundary diffusion coefficients.
Due to normal growth, which requires additional material, the lateral propagation rate in uncovered films becomes lower compared to that in the covered films where normal growth is absent. 05 10 15 20 25 0 0.5 1 1.5 2 2.5 t1/2 (h1/2 ) xA1 ( m) H=90 nm; a=18 nm H=90 nm; a=40 nm H=50 nm; a=18 nm H=180 nm; a=18 nm 1 2 m) 0 5 10 15 20 25 30 35 40 0 0.5 1 1.5 2 2.5 t 1/2 (h 1/2) xA2 ( m) H=90 nm; a=18 nm H=90 nm; a=40 nm H=50 nm; a=18 nm H=180 nm; a=18nm 2 1 m) Fig. 4.
Specific feature of nano-grained materials consists in small length of the B-zone in comparison with the zone A: the smaller grain size, the shorter is the B-zone.
Acknowledgements This research was supported by a grant from the Ministry of Science and Technology of Israel (grant # 3-2820) and the Ministry of Education and Science of Ukraine (grant # M/257-2006) References [1] T.
Predel: Journal de Physique.
Due to normal growth, which requires additional material, the lateral propagation rate in uncovered films becomes lower compared to that in the covered films where normal growth is absent. 05 10 15 20 25 0 0.5 1 1.5 2 2.5 t1/2 (h1/2 ) xA1 ( m) H=90 nm; a=18 nm H=90 nm; a=40 nm H=50 nm; a=18 nm H=180 nm; a=18 nm 1 2 m) 0 5 10 15 20 25 30 35 40 0 0.5 1 1.5 2 2.5 t 1/2 (h 1/2) xA2 ( m) H=90 nm; a=18 nm H=90 nm; a=40 nm H=50 nm; a=18 nm H=180 nm; a=18nm 2 1 m) Fig. 4.
Specific feature of nano-grained materials consists in small length of the B-zone in comparison with the zone A: the smaller grain size, the shorter is the B-zone.
Acknowledgements This research was supported by a grant from the Ministry of Science and Technology of Israel (grant # 3-2820) and the Ministry of Education and Science of Ukraine (grant # M/257-2006) References [1] T.
Predel: Journal de Physique.
Online since: April 2010
Authors: Simon C. Hopkins, Bartek A. Glowacki, Ludovic Thilly, Marco Di Michiel, Ian Pong, Christian Scheuerlein, Carmine Senatore, Alexandre Gerardin, Luc-Rene Oberli, Guillaume Geandier, Luca Bottura
Glowacki5, j, Luca Bottura
1, k
1
CERN, CH-1211 Geneva 23, Switzerland
2
Département de Physique de la Matière Condensée & MaNEP, Université de Genève, 24, quai
Ernest-Ansermet, CH-1211 Genève-4, Switzerland
3
Université de Poitiers, PHYMAT, SP2MI, F-86962 Futuroscope, France
4
ESRF, 6 rue Jules Horowitz, F-38000 Grenoble, France
5
Applied Superconductivity and Cryoscience Group, Department of Materials Science and
Metallurgy, Pembroke Street, University of Cambridge, CB2 3QZ, United Kingdom
6
Synchrotron SOLEIL, 91192 GIF-sur-YVETTE CEDEX France
a
ian.pong@cern.ch, bchristian.scheuerlein@cern.ch, ccarmine.senatore@unige.ch,
d
ludovic.thilly@univ-poitiers.fr, emarco.di_michiel@esrf.fr, falexandre.gerardin@cern.ch,
g
sch29@cam.ac.uk, hluc-rene.oberli@cern.ch, igeandier@synchrotron-soleil.fr,
jbag10@cam.ac.uk, kluca.bottura@cern.ch
Keywords: Cu-Ti, intermetallic compound, Nb-Ti, superconductor, LHC, ESRF, in situ XRD, in situ
resistometry, RRR, superconducting
The starting material is the LHC 02 reference wire, with approximately 6500 roughly circular Nb-47 wt% Ti filaments embedded in an OFHC Cu matrix.
Biner: Journal of Materials Science Vol. 28, (1993), p. 4623.
The starting material is the LHC 02 reference wire, with approximately 6500 roughly circular Nb-47 wt% Ti filaments embedded in an OFHC Cu matrix.
Biner: Journal of Materials Science Vol. 28, (1993), p. 4623.
Online since: September 2013
Authors: Qiu Jing Zhou, Yi Liu, Guo Xin Zhang
Prediction of and Early Warning for Deformation and Stress in the Xiaowan Arch Dam during the First Impounding Stage
ZHOU Qiujing 1, a, ZHANG Guoxin 1, b and LIU Yi1, c
1 Department of Structures and Materials, China Institute of Water Resources and Hydropower Research, Beijing 100038, China
azhouqj@iwhr.com, bzhanggx@iwhr.com, cliuyi@iwhr.com
Keywords: High arch dams, Prediction and early warning, Deformation, Stress, First impounding stage
Abstract.
Inversion analysis should also be conducted on the thermal parameters of the actual performance of dam concrete according to the measured air temperature, water temperature, sun exposure, other boundary conditions, and the thermal parameters of concrete materials obtained in material tests.
Acknowledgments This work was financially supported by the National Natural Science Foundation of China (50909105), the National Basic Research Program of China (973 Program) (2013CB035904, 2013CB036406), the National “Twelfth Five-Year” Plan for Science and Technology Support (SQ2013BAJY4138B02), the Governmental Public Industry Research Special Funds for Projects of MWR (201201050), and the Special Research Funds of IWHR (1361/1353/1169/1309).
[7] Li Zan: Study on cracks at the heel of the arch dam of shimen project, Journal of Hydraulic Engineering, 11, (1999), p.61-65
Inversion analysis should also be conducted on the thermal parameters of the actual performance of dam concrete according to the measured air temperature, water temperature, sun exposure, other boundary conditions, and the thermal parameters of concrete materials obtained in material tests.
Acknowledgments This work was financially supported by the National Natural Science Foundation of China (50909105), the National Basic Research Program of China (973 Program) (2013CB035904, 2013CB036406), the National “Twelfth Five-Year” Plan for Science and Technology Support (SQ2013BAJY4138B02), the Governmental Public Industry Research Special Funds for Projects of MWR (201201050), and the Special Research Funds of IWHR (1361/1353/1169/1309).
[7] Li Zan: Study on cracks at the heel of the arch dam of shimen project, Journal of Hydraulic Engineering, 11, (1999), p.61-65
Online since: April 2022
Authors: Naho Itagaki, Kazunori Koga, Kunihiro Kamataki, Masaharu Shiratani, Pankaj Attri, Fadzai Lesley Chawarambwa, Tika Erna Putri
Moreover, Pt is a highly expensive rare metal, and this challenge has spurred research in alternative counter electrode materials and new Pt depositions methods [11].
Experimental Methods Materials.
All materials were used as purchased without further modifications.
Counter electrodes for DSC: Application of functional materials as catalysts, Inorg.
Talib, The effect of spin coating rate on the microstructure, grain size, surface roughness and thickness of Ba0.6Sr0.4TiO3 thin film prepared by the sol-gel process., Materials Science-Poland, Vol. 25, No. 3, (2007) 657-662
Experimental Methods Materials.
All materials were used as purchased without further modifications.
Counter electrodes for DSC: Application of functional materials as catalysts, Inorg.
Talib, The effect of spin coating rate on the microstructure, grain size, surface roughness and thickness of Ba0.6Sr0.4TiO3 thin film prepared by the sol-gel process., Materials Science-Poland, Vol. 25, No. 3, (2007) 657-662
Online since: October 2006
Authors: S.J. Bull, Jinju Chen
Combining the numerical simulations and
calibration on realistic materials, the plastic work can be estimated and the irreversible work can be
easily calculated from the load-displacement curve.
The interfacial toughness can be estimated by treating the interface as a homogeneous material with the Young's modulus and hardness as composite parameters of the coating and substrate so that linear fracture mechanics for brittle materials can be applied.
Marshall et al [43] proposed a model to relate the toughness of brittle bulk materials to the depth where lateral cracks occur and the crack driving force Pr due to the residual stress during unloading.
McPherson, Materials Science Research, 14 (1981)619 16.
Evans Journal of Applied Physics, 56(1984) 2632 40.
The interfacial toughness can be estimated by treating the interface as a homogeneous material with the Young's modulus and hardness as composite parameters of the coating and substrate so that linear fracture mechanics for brittle materials can be applied.
Marshall et al [43] proposed a model to relate the toughness of brittle bulk materials to the depth where lateral cracks occur and the crack driving force Pr due to the residual stress during unloading.
McPherson, Materials Science Research, 14 (1981)619 16.
Evans Journal of Applied Physics, 56(1984) 2632 40.
Online since: February 2025
Authors: Nathaniel Wambebe, Adindu C. Kingsley, Sammy Joel Panwal
Kingsley3
1Public Health Dept, Faculty of Health Sciences, National Open University of Nigeria.
2School of Energy and Environmental Engineering, University of Science & Technology Beijing, China.
3Institute of Natural Resources, Environment and Sustainability, University of Port Harcourt.
Methods and Materials Study Design and Location This study adopted a cross-sectional design, similar to those used by Hautekiet et al, (2022) [9].
Kato, ‘Leonardo Electronic Journal of Practices and Technologies Contributions of Vehicular Traffic to Carbon Dioxide Emissions in Kaduna and Abuja, Northern Nigeria’, 2006, [Online].
Pius O, ‘Evaluation of the meteorological, air quality in the urban and rural areas of rivers state, South-South, Nigeria’, MOJ Ecology & Environmental Sciences, vol. 9, no. 2, pp. 46–53, Mar. 2024, doi: 10.15406/mojes.2024.09.00306
, PLoS One, vol. 10, no. 3, Mar. 2015, doi: 10.1371/journal.pone.0121573
Methods and Materials Study Design and Location This study adopted a cross-sectional design, similar to those used by Hautekiet et al, (2022) [9].
Kato, ‘Leonardo Electronic Journal of Practices and Technologies Contributions of Vehicular Traffic to Carbon Dioxide Emissions in Kaduna and Abuja, Northern Nigeria’, 2006, [Online].
Pius O, ‘Evaluation of the meteorological, air quality in the urban and rural areas of rivers state, South-South, Nigeria’, MOJ Ecology & Environmental Sciences, vol. 9, no. 2, pp. 46–53, Mar. 2024, doi: 10.15406/mojes.2024.09.00306
, PLoS One, vol. 10, no. 3, Mar. 2015, doi: 10.1371/journal.pone.0121573