Synthesis Route towards Fine and Monodisperse Ni Nanoparticles via Hot-Injection Approach

N.R. Nik Roselina; Aziz Azizan; Koay Mei Hyie; C.M.  Mardziah; Salmiah Kasolang; Siti Khadijah Alias; Z. Salleh

doi:10.4028/www.scientific.net/AMM.393.146

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HomeApplied Mechanics and MaterialsApplied Mechanics and Materials Vol. 393Synthesis Route towards Fine and Monodisperse Ni...

Synthesis Route towards Fine and Monodisperse Ni Nanoparticles via Hot-Injection Approach

Abstract:

Manipulation of adding sequences have been found to influence the reaction rate, thus made it easier to produced controllable Ni nanoparticles. Hot-injection approach shown capability to significantly reduce the production time of Ni nanoparticles compared to the conventional one-pot synthesis. With minor modification on conventional polyol method, narrow, monodispersed and highly yield spherical nickel (Ni) nanoparticles were successfully produced at synthesis temperature of 60°C. Three mixing methods were investigated to study its efficiency towards producing rapid and narrower size distribution of Ni nanoparticles. Reduction processes were proposed each of the method. As-synthesized Ni nanoparticles were characterized with Transmission Electron Microscopy (TEM), Scanning Transmission Electron Microscopy (STEM) and Fourier transform infrared spectroscopy (FTIR) to analyze the size, morphology and interaction of reactants. Fine particles size distribution revealed that when hydrazine was first heated, reaction rate improved tremendously.

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Periodical:

Applied Mechanics and Materials (Volume 393)

Pages:

146-151

DOI:

https://doi.org/10.4028/www.scientific.net/AMM.393.146

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Online since:

September 2013

Authors:

N.R. Nik Roselina, Aziz Azizan, Koay Mei Hyie, C.M. Mardziah, Salmiah Kasolang, Siti Khadijah Alias, Z. Salleh

Keywords:

Hot-Injection, Nanoparticle, Nickel, Synthesis

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