Detecting PAEs in Bottled Water by SPE-LC/QQQ

Yu Zi Liu; Ying Hao Xing; Jun Wu

doi:10.4028/www.scientific.net/AMM.469.444

Paper Titles

Dynamics Research of Time-Temperature Indicating System Based on Alkaline Lipase
p.422

A Study on Migration of Contamination from Paper Cups to Ethanol by HPLC
p.431

Study on the Migration Process of Food Packaging Materials
p.436

Correlation between Partition Coefficients Food Simulant/Paper, K_{F, P}, and Octanol/Water, K_{O,W -}A New Approach in Support of Migration Modeling and Compliance Testing
p.440

Detecting PAEs in Bottled Water by SPE-LC/QQQ
p.444

Study on Formaldehyde Migration Rules in Products of Tripolycyanamide for Food Packaging
p.450

Researching the Influence of Repeated Using to the Migration of Residue Bisphenol a from Polycarbonate with GC-MS Technology
p.454

Determination of 15 PAEs in Fatty Food by SPE-GC/MS
p.458

Application of Internet of Things Technology in Tracing to Food Source
p.467

HomeApplied Mechanics and MaterialsApplied Mechanics and Materials Vol. 469Detecting PAEs in Bottled Water by SPE-LC/QQQ

Detecting PAEs in Bottled Water by SPE-LC/QQQ

Abstract:

In this study, High Performance Liquid Chromatography (HPLC), combined with Triple Quadruple mass Spectrometry (QQQ) were developed and applied in the analysis of 16 phthalic acid esters (PAEs) in the common drinking water. Qualitative and quantitative analysis were carried out by Multiple Reaction Monitoring (MRM). The method, combined with Solid Phase Extraction, was established to detect the PAEs in drinking water. As showed by the results, 16 PAEs had a good linearity in the range of 1.14~101.4μg/L, with correlation coefficient between 0.996~0.999. The mean recoveries were in the range of 87.53~131.37%, with the relative standard deviation be 0.71~5.09%. The limit of quantification (LOQ) of 16 PAEs were between 1.14~32.51μg/L, with the limit of detection (LOD) be 0.34~10.67μg/L. There were five PAEs which were detected in the range of <1.7~17.2μg/L in bottled water. Some products have some PAEs which havent been shown in the national or the international standard of the drinking water.